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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
15802-62-7
合成路线
（共 9 条）
15802-62-7
+
17356-08-0
→
反应条件
123043-88-9
反应条件
1: thiourea With 1-methyl-pyrrolidin-2-one; resin bound 4-(benzyloxy)benzyl chloride T=75°C; Alkylation; 16 h; solid phase reaction; 2: (Z)-2-benzylidene-3-oxobutanoic acid ethyl ester With 1-methyl-pyrrolidin-2-one; caesium carbonate T=90°C; Cycloaddition; 16 h; solid phase reaction; 3: With trifluoroacetic acid; ethanethiol in dichloromethane T=20°C; Cleavage; 16 h;
参考文献
Kappe, C. Oliver
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 1 p. 49 - 51
1118-66-7
4-氨基-3-戊烯-2-酮
+
15802-62-7
→
反应条件
20970-67-6
+
20970-69-8
乙基5-乙酰基-2,6-二甲基-4-苯基-1,4-二氢-3-吡啶羧酸酯
+
1165-06-6
2,6-二甲基-4-苯基-1,4-二氢吡啶-3,5-二羧酸二乙酯
反应条件
in methanol 16 h; Heating;
参考文献
Memarian, Hamid R.; Abdoli-Senejani, Masumeh; Doepp, Dietrich
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 1 p. 50 - 56
15802-62-7
+
17356-08-0
→
反应条件
123237-03-6
反应条件
1: thiourea With 1-methyl-pyrrolidin-2-one; resin bound 4-(benzyloxy)benzyl chloride T=75°C; Alkylation; 16 h; solid phase reaction; 2: (Z)-2-benzylidene-3-oxobutanoic acid ethyl ester With 1-methyl-pyrrolidin-2-one; caesium carbonate T=90°C; Cycloaddition; 16 h; solid phase reaction; 3: With acetic acid in 1,4-dioxane; ethanol Cleavage; 16 h; Heating;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 1 p. 49 - 51
15802-62-7
+
17356-08-0
→
反应条件
123237-03-6
反应条件
1: thiourea With 1-methyl-pyrrolidin-2-one; resin bound 4-(benzyloxy)benzyl chloride T=75°C; Alkylation; 16 h; solid phase reaction; 2: (Z)-2-benzylidene-3-oxobutanoic acid ethyl ester With 1-methyl-pyrrolidin-2-one; caesium carbonate T=90°C; Cycloaddition; 16 h; solid phase reaction; 3: With acetic acid in 1,4-dioxane; ethanol Cleavage; 16 h; Heating;
参考文献
Kappe, C. Oliver
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 1 p. 49 - 51
1118-66-7
4-氨基-3-戊烯-2-酮
+
15802-62-7
→
反应条件
20970-67-6
+
20970-69-8
乙基5-乙酰基-2,6-二甲基-4-苯基-1,4-二氢-3-吡啶羧酸酯
+
1165-06-6
2,6-二甲基-4-苯基-1,4-二氢吡啶-3,5-二羧酸二乙酯
反应条件
in methanol 16 h; Heating;
参考文献
Memarian, Hamid R.; Abdoli-Senejani, Masumeh; Doepp, Dietrich
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 1 p. 50 - 56
1118-66-7
4-氨基-3-戊烯-2-酮
+
15802-62-7
→
反应条件
20970-67-6
+
20970-69-8
乙基5-乙酰基-2,6-二甲基-4-苯基-1,4-二氢-3-吡啶羧酸酯
+
1165-06-6
2,6-二甲基-4-苯基-1,4-二氢吡啶-3,5-二羧酸二乙酯
反应条件
in methanol 16 h; Heating;
参考文献
Memarian, Hamid R.; Abdoli-Senejani, Masumeh; Doepp, Dietrich
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 1 p. 50 - 56
15802-62-7
+
109-77-3
丙二腈
→
反应条件
72568-47-9
6-氨基-5-氰基-2-甲基-4-苯基-4H-吡喃-3-羧酸乙酯
反应条件
piperidine in ethanol Ambient temperature;
参考文献
Soto, Jose L.; Seoane, Carlos; Martin, Nazario; Quinteiro, Margarita
Heterocycles, 1984 , vol. 22, # 1 p. 1 - 6
15802-62-7
+
75-08-1
乙硫醇
→
反应条件
7334-52-3
反应条件
aluminium trichloride T=0°C; 0.33 h;
参考文献
Fuji, Kaoru; Kawabata, Takeo; Node, Manabu; Fujita, Eiich
Tetrahedron Letters, 1981 , vol. 22, p. 875 - 878
15802-62-7
+
614-47-1
反式-查耳酮
→
反应条件
6265-29-8
+
6287-66-7
反应条件
piperidine in ethanol Michael addition; 0.133333 h; microwave irradiation;
参考文献
Laskar, Dhrubojyoti D.; Prajapati, Dipak; Sandhu, Jagir S.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 1 p. 135 - 139
