3,5-二炔-1,8-辛二醇合成路线 （共 9 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-butylamine in benzene T=45°C; Sonogashira Cross-Coupling; 0.75 h; Inert atmosphere; Further stages;
参考文献
Yalagala, Ravi Shekar; Zhou, Ningzhang; Yan, Hongbin
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1883 - 1885
反应条件
copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in benzene T=20°C; Sonogashira reaction; 2 h;
参考文献
Lee, Hee Bong; Huh, Dal Ho; Oh, Joon Seok; Min, Gwan-Hong; Kim, Byung Hyun; Lee, Dong Hwal; Hwang, Jae Kwang; Kim, Young Gyu
Tetrahedron, 2001 , vol. 57, # 39 p. 8283 - 8290
反应条件
piperidine; copper (II) acetate monohydrate in dichloromethane T=25°C; 3 h; air;
参考文献
Balaraman, Kaluvu; Kesavan, Venkitasamy
Synthesis, 2010 , # 20 art. no. Z15010SS, p. 3461 - 3466
反应条件
copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in ethyl acetate T=20°C; Sonogashira reaction; 5 h;
参考文献
Lee, Hee Bong; Huh, Dal Ho; Oh, Joon Seok; Min, Gwan-Hong; Kim, Byung Hyun; Lee, Dong Hwal; Hwang, Jae Kwang; Kim, Young Gyu
Tetrahedron, 2001 , vol. 57, # 39 p. 8283 - 8290
反应条件
copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride T=60°C; Sonogashira reaction; 2 h;
参考文献
Pereira, Raquel; Iglesias, Beatriz; De Lera, Angel R
Tetrahedron, 2001 , vol. 57, # 37 p. 7871 - 7881
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine in acetonitrile Sonogashira coupling; 3 h; Reflux;
参考文献
Bouchikhi, Fadoua; Anizon, Fabrice; Moreau, Pascale
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 6 p. 2705 - 2710
参考文献
Bowden et al.
Journal of the Chemical Society, 1947 , p. 1582
反应条件
platinum(IV) oxide; acetic acid ester Hydrogenation;
参考文献
Bowden et al.
Journal of the Chemical Society, 1947 , p. 1582
参考文献
Bowden et al.
Journal of the Chemical Society, 1947 , p. 1582
