2-氟-2’,3’,5’-三乙酰氧基腺苷合成路线 （共 4 条）
反应条件
tert.-butylnitrite; hydrogen fluoride in pyridine T=-30 - -20°C; 0.166667 h;
参考文献
Robins; Uznanski
Canadian Journal of Chemistry, 1981 , vol. 59, # 17 p. 2608 - 2611
反应条件
palladium 10 on activated carbon; hydrogen; trifluoroacetic acid in ethyl acetate
参考文献
Berzin; Dorofeeva; Leonov; Miroshnikov
Russian Journal of Bioorganic Chemistry, 2009 , vol. 35, # 2 p. 193 - 196
反应条件
in ethylene glycol dimethyl ether 0.25 h; Ambient temperature;
参考文献
Robins; Uznanski
Canadian Journal of Chemistry, 1981 , vol. 59, # 17 p. 2608 - 2611
反应条件
1: 66 percent / HF (60percent), tert-butyl nitrite (TBN) / pyridine / 0.02 h / -30 °C 2: 85 percent / 1,2-dimethoxy-ethane / 0.25 h / Ambient temperature View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 59, # 17 p. 2608 - 2611
