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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
158146-85-1
合成路线
（共 10 条）
→
反应条件
158146-85-1
反应条件
hydrogenchloride; sodium nitrite in water
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5698699 A1, 1997 ;
288-88-0
1,2,4-三氮唑
+
153394-50-4
→
反应条件
158146-85-1
反应条件
in N,N-dimethyl-formamide
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5719157 A1, 1998 ;
288-88-0
1,2,4-三氮唑
+
7285-11-2
+
153394-50-4
→
反应条件
158146-85-1
反应条件
in water; N,N-dimethyl-formamide
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5698699 A1, 1997 ;
288-88-0
1,2,4-三氮唑
+
153394-50-4
→
反应条件
反应条件
sodium hydride in N,N-dimethyl-formamide T=80°C;
参考文献
Mizuno, Masahiro; Inagaki, Atsushi; Yamashita, Makoto; Soma, Norie; Maeda, Yoshiharu; Nakatani, Hiroshi
Tetrahedron, 2006 , vol. 62, # 17 p. 4065 - 4070
638-07-3
4-氯乙酰乙酸乙酯
→
反应条件
158146-85-1
反应条件
1.1: ethanol / 3 h / 77 - 80 °C 1.2: 88 percent / triethylamine / ethanol / 1 h / 5 - 15 °C 2.1: 60 percent / NaH / dimethylformamide / 80 °C View Scheme
参考文献
Mizuno, Masahiro; Inagaki, Atsushi; Yamashita, Makoto; Soma, Norie; Maeda, Yoshiharu; Nakatani, Hiroshi
Tetrahedron, 2006 , vol. 62, # 17 p. 4065 - 4070
881-70-9
二甲氧基乙酰苯胺
→
反应条件
158146-85-1
反应条件
1.1: 99 percent / phosphorus oxychloride; tin(IV) chloride / CH2Cl2 / 12 h / Heating 2.1: 94 percent / hydrochloric acid / isobutanol / 2 h / Heating 3.1: ethanol / 3 h / 77 - 80 °C 3.2: 88 percent / triethylamine / ethanol / 1 h / 5 - 15 °C 4.1: 60 percent / NaH / dimethylformamide / 80 °C View Scheme
参考文献
Mizuno, Masahiro; Inagaki, Atsushi; Yamashita, Makoto; Soma, Norie; Maeda, Yoshiharu; Nakatani, Hiroshi
Tetrahedron, 2006 , vol. 62, # 17 p. 4065 - 4070
6315-89-5
3,4-二甲氧基苯胺
→
反应条件
158146-85-1
反应条件
1.1: 89 percent / sodium hydroxide / H2O / 5 - 60 °C 2.1: 99 percent / phosphorus oxychloride; tin(IV) chloride / CH2Cl2 / 12 h / Heating 3.1: 94 percent / hydrochloric acid / isobutanol / 2 h / Heating 4.1: ethanol / 3 h / 77 - 80 °C 4.2: 88 percent / triethylamine / ethanol / 1 h / 5 - 15 °C 5.1: 60 percent / NaH / dimethylformamide / 80 °C View Scheme
参考文献
Mizuno, Masahiro; Inagaki, Atsushi; Yamashita, Makoto; Soma, Norie; Maeda, Yoshiharu; Nakatani, Hiroshi
Tetrahedron, 2006 , vol. 62, # 17 p. 4065 - 4070
189001-13-6
→
反应条件
158146-85-1
反应条件
1.1: 94 percent / hydrochloric acid / isobutanol / 2 h / Heating 2.1: ethanol / 3 h / 77 - 80 °C 2.2: 88 percent / triethylamine / ethanol / 1 h / 5 - 15 °C 3.1: 60 percent / NaH / dimethylformamide / 80 °C View Scheme
参考文献
Mizuno, Masahiro; Inagaki, Atsushi; Yamashita, Makoto; Soma, Norie; Maeda, Yoshiharu; Nakatani, Hiroshi
Tetrahedron, 2006 , vol. 62, # 17 p. 4065 - 4070
153394-55-9
→
反应条件
158146-85-1
反应条件
1: 50 percent / H2SO4; AcOH / 90 °C 2: 60 percent / NaH / dimethylformamide / 80 °C View Scheme
参考文献
Baba, Atsuo; Kawamura, Noriaki; Makino, Haruhiko; Ohta, Yoshikazu; Taketomi, Shigehisa; Sohda, Takashi
Journal of Medicinal Chemistry, 1996 , vol. 39, # 26 p. 5176 - 5182
153394-50-4
→
反应条件
158146-85-1
反应条件
1.1: 79 percent / sodium bromide / dimethylformamide / 5 h / 63 - 67 °C 2.1: hydrochloric acid; sodium nitrite / H2O / 3 h / 23 °C 2.2: 94 percent / sodium hydroxide / H2O / 10 - 20 °C / pH 6.7 View Scheme
参考文献
Mizuno, Masahiro; Inagaki, Atsushi; Yamashita, Makoto; Soma, Norie; Maeda, Yoshiharu; Nakatani, Hiroshi
Tetrahedron, 2006 , vol. 62, # 17 p. 4065 - 4070
