反应条件
1: acetylacetone With sodium hydride in tetrahydrofuran T=0°C; 0.333333 h; Inert atmosphere; 2: With n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.166667 h; Inert atmosphere; 3: 1,6-dibromo-n-hexane in tetrahydrofuran; hexane T=0 - 20°C; 4.33333 h; Inert atmosphere;
参考文献
Maurer, Christian; Pittenauer, Ernst; Du, Van An; Allmaier, Guenter; Schubert, Ulrich
Dalton Transactions, 2012 , vol. 41, # 8 p. 2346 - 2353