2,7-二溴-1,6-甲桥[10]环轮烯合成路线 （共 6 条）
反应条件
N-bromosuccinmide in dichloromethane T=40°C; 4 h;
参考文献
Takahashi, Kazuko; Ohnishi, Keiichi; Takase, Kahei
Chemistry Letters, 1985 , p. 1079 - 1082
反应条件
N-bromosuccinmide in dichloromethane 0.5 h; Ambient temperature;
参考文献
Takahashi, Kazuko; Ohnishi, Keiichi; Takase, Kahei
Chemistry Letters, 1985 , p. 1079 - 1082
参考文献
Klenk,H. et al.
Chemische Berichte, 1976 , vol. 109, p. 777 - 787
反应条件
1: 93 percent / NBS / CH2Cl2 / 0 °C 2: 93 percent / NBS / CH2Cl2 / 0.5 h / Ambient temperature View Scheme
参考文献
Takahashi, Kazuko; Ohnishi, Keiichi; Takase, Kahei
Chemistry Letters, 1985 , p. 1079 - 1082
反应条件
n-butyllithium
1) ether, n-hexane, 50 min, -20 deg C, 2) ether, n-hexane, 0.5 h, 0 deg C; 4 h, r.t.; Yield given. Multistep reaction;
参考文献
Neidlein, Richard; Zeiner, Hartmut
Chemische Berichte, 1982 , vol. 115, # 4 p. 1409 - 1417
反应条件
in methanol
T=30°C; Substitution; 48 h;
参考文献
De Farias Dias, Aderson; Helwig, Thomas; Lex, Johann; Miller, Joseph; Schmickler, Hans
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 13 p. 2083 - 2089
