(1E)-1-(4-氟苯基)-N-羟基乙烷亚胺合成路线 （共 4 条）
反应条件
2,4,6-trichloro-1,3,5-triazine; zinc(II) chloride in acetonitrile Beckmann rearrangement; 2 h; Heating;
参考文献
Furuya, Yoshiro; Ishihara, Kazuaki; Yamamoto, Hisashi
Journal of the American Chemical Society, 2005 , vol. 127, # 32 p. 11240 - 11241
反应条件
1: With (Ph)2SiH2; silver trifluoromethanesulfonate in tetrahydrofuran T=20°C; 25 h; 2: With hydrogenchloride in tetrahydrofuran; methanol Further stages. Title compound not separated from byproducts.;
参考文献
Chemical Communications, , # 22 p. 2360 - 2361
反应条件
1: With (Ph)2SiH2; silver trifluoromethanesulfonate in tetrahydrofuran T=20°C; 25 h; 2: With hydrogenchloride in tetrahydrofuran; methanol Further stages. Title compound not separated from byproducts.;
参考文献
Pakulski, Marcin M.; Mahato, Sanjit K.; Bosiak, Mariusz J.; Krzeminski, Marek P.; Zaidlewicz, Marek
Tetrahedron Asymmetry, 2012 , vol. 23, # 9 p. 716 - 721
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C 1.2: 18 h / 20 °C 2.1: C19H23BNO3(1-)*H(1+); borane-THF / 1,4-dioxane / 72 h / |Inert atmosphere View Scheme
参考文献
Ou, Wenhua; Espinosa, Sandraliz; Melendez, Hector J.; Farre, Silvia M.; Alvarez, Jaime L.; Torres, Valerie; Martinez, Ileanne; Santiago, Kiara M.; Ortiz-Marciales, Margarita
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5314 - 5327
