7-甲氧基-1-萘并ni三le合成路线 （共 17 条）
反应条件
1: With zinc(II) iodide in toluene T=45°C; 3.33333 h; Reflux; 2: With pyridine; trichlorophosphate in toluene T=35°C; Reflux; 3: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene 2 h; Reflux;
参考文献
Hartmann, Rolf; Frotscher, Martin; Oberwinkler, Sandrine; Ziegler, Erika; Messinger, Josef; Thole, Heinrich-Hubert
Patent: US2010/204234 A1, 2010 ;
Location in patent: Page/Page column 14 ;
US 20100204234 A1
反应条件
palladium on activated charcoal T=250°C; 6 h;
参考文献
Hayashi, Takashi; Miyahara, Takashi; Aoyama, Yasunori; Nonoguchi, Masanori; Ogoshi, Hisanobu
Chemistry Letters, 1994 , # 9 p. 1749 - 1752
反应条件
in 1-methyl-pyrrolidin-2-one T=150°C; Rosenmund-van Braun Cyanation; 2 h;
参考文献
Kandagatla, Bhaskar; Raju, Vetukuri Venkata Naga Kali Vara Prasada; Reddy, Ganta Madhusudhan; Rao, Sirigiri Chandrakanth; Iqbal, Javed; Bandichhor, Rakeshwar; Oruganti, Srinivas
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7125 - 7127
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
参考文献
Wyeth
Patent: US2003/181519 A1, 2003 ;
反应条件
1.1: ZnI2 / benzene / 20 °C 1.2: POCl3; pyridine / benzene / 6 h / Heating 2.1: p-cymene / Pd/C / Heating View Scheme
参考文献
Hayashi, Takashi; Miyahara, Takashi; Aoyama, Yasunori; Nonoguchi, Masanori; Ogoshi, Hisanobu
Chemistry Letters, 1994 , # 9 p. 1749 - 1752
反应条件
1.1: potassium carbonate / acetone / 0.25 h / 20 °C 1.2: 3 h / 20 °C 2.1: 1-methyl-pyrrolidin-2-one / 2 h / 150 °C View Scheme
参考文献
Kandagatla, Bhaskar; Raju, Vetukuri Venkata Naga Kali Vara Prasada; Reddy, Ganta Madhusudhan; Rao, Sirigiri Chandrakanth; Iqbal, Javed; Bandichhor, Rakeshwar; Oruganti, Srinivas
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7125 - 7127
反应条件
1.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 - 5 °C 1.2: 2.5 h / 0 - 5 °C 2.1: potassium carbonate / acetone / 0.25 h / 20 °C 2.2: 3 h / 20 °C 3.1: 1-methyl-pyrrolidin-2-one / 2 h / 150 °C View Scheme
参考文献
Kandagatla, Bhaskar; Raju, Vetukuri Venkata Naga Kali Vara Prasada; Reddy, Ganta Madhusudhan; Rao, Sirigiri Chandrakanth; Iqbal, Javed; Bandichhor, Rakeshwar; Oruganti, Srinivas
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7125 - 7127
反应条件
in water; acetone; tert-butyl alcohol Irradiation;
参考文献
Den Heijer,J. et al.
Tetrahedron, 1977 , vol. 33, p. 779 - 786
反应条件
sodium cyanide in dimethyl sulfoxide T=160 - 170°C; 12 h;
参考文献
Tolbert, Laren M.; Haubrich, Jeanne E.
Journal of the American Chemical Society, 1994 , vol. 116, # 23 p. 10593 - 10600
参考文献
Wyeth
Patent: US2003/181519 A1, 2003 ;
