2-丁基-5-氯-1H-咪唑合成路线 （共 8 条）
反应条件
sodium hydroxide in trichlorophosphate
参考文献
Lonza Ltd.
Patent: US5484939 A1, 1996 ;
反应条件
tetrachloromethane; triphenylphosphine in acetonitrile T=45°C; 16 h;
参考文献
Zhong, Yong-Li; Lee, Jaemoon; Reamer, Robert A.; Askin, David
Organic Letters, 2004 , vol. 6, # 6 p. 929 - 931
反应条件
2: 31 percent / POCl3 / chlorobenzene / 2 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 22 p. 8084 - 8089
反应条件
1: 190.8 g / HCl / dibutyl ether / 144 h / 4 °C 2: 95 percent / NaOH / methanol; toluene / 3 h / 20 °C 3: 31 percent / POCl3 / chlorobenzene / 2 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 22 p. 8084 - 8089
反应条件
1: 95 percent / NaOH / methanol; toluene / 3 h / 20 °C 2: 31 percent / POCl3 / chlorobenzene / 2 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 22 p. 8084 - 8089
反应条件
1: 40 percent / 24 h / -10 °C 2: 31 percent / POCl3 / chlorobenzene / 2 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 22 p. 8084 - 8089
反应条件
trichlorophosphate in chlorobenzene T=100°C; Formylation; Vilsmeier reaction; 4 h;
参考文献
Griffiths, Gareth J.; Hauck, Michael B.; Imwinkelried, Rene; Kohr, Joerg; Roten, Conrad A.; Stucky, Gerhard C.; Gosteli, Jacques
Journal of Organic Chemistry, 1999 , vol. 64, # 22 p. 8084 - 8089
反应条件
1: Et3N / chlorobenzene / Heating 2: H2O / Acid hydrolysis View Scheme
参考文献
Griffiths, Gareth J.; Hauck, Michael B.; Imwinkelried, Rene; Kohr, Joerg; Roten, Conrad A.; Stucky, Gerhard C.; Gosteli, Jacques
Journal of Organic Chemistry, 1999 , vol. 64, # 22 p. 8084 - 8089
