甲基(苯基)亚膦基氯化物合成路线 （共 11 条）
反应条件
magnesium Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 60, # 16 p. 5190 - 5208
反应条件
hydrogenchloride in Petroleum ether
参考文献
Bestmann, Hans Juergen; Lienert, Juergen; Heid, Eckard
Chemische Berichte, 1982 , vol. 115, # 12 p. 3875 - 3879
反应条件
triphenyl phosphite
Heating;
参考文献
Mikolajczyk, Marian; Graczyk, Piotr P.; Wieczorek, Michal W.
Journal of Organic Chemistry, 1994 , vol. 59, # 7 p. 1672 - 1693
反应条件
chloro-diphenylphosphine
2 h;
参考文献
Wolfsberger, W
Journal of Organometallic Chemistry, 1986 , vol. 317, p. 167 - 174
反应条件
1,2,2-trichloro-1,1,2-trichloro-ethane in dichloromethane
参考文献
Appel,R. et al.
Chemische Berichte, 1977 , vol. 110, p. 376 - 378
反应条件
1: 85 percent / diethyl ether / 1 h / -40 °C
2: HCl / diethyl ether / 1 h / 0 °C
View Scheme
参考文献
Andersen; Ramsden; Che; Parvez; Keay
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7478 - 7486
反应条件
1: 89.70 g / diethyl ether / 12 h / Ambient temperature
2: 51 percent / diethyl ether / 1) 1 h, r.t., 2) 1 h, reflux
3: 78 percent / HCl / petroleum ether
View Scheme
参考文献
Bestmann, Hans Juergen; Lienert, Juergen; Heid, Eckard
Chemische Berichte, 1982 , vol. 115, # 12 p. 3875 - 3879
反应条件
1: 51 percent / diethyl ether / 1) 1 h, r.t., 2) 1 h, reflux
2: 78 percent / HCl / petroleum ether
View Scheme
参考文献
Bestmann, Hans Juergen; Lienert, Juergen; Heid, Eckard
Chemische Berichte, 1982 , vol. 115, # 12 p. 3875 - 3879
参考文献
Lindner, Ekkehard; Merkle, Ralf Dieter; Mayer, Hermann August
Chemische Berichte, 1986 , vol. 119, # 2 p. 645 - 658
反应条件
pyridine
1.) THF, ether, -70 deg C to -10 deg C, 2.) THF, ether, RT, 72 h; Yield given. Multistep reaction;
参考文献
Chodkiewicz, W.; Guillerm, D.; Jore, D.; Mathieu, E.; Wodzki, W.
Journal of Organometallic Chemistry, 1984 , vol. 269, # 2 p. 107 - 114
