2-苯基-4-硝基苯甲醚合成路线 （共 19 条）
反应条件
1: PTAS With tetrabutyl ammonium fluoride in tetrahydrofuran; water T=20°C; 1 h; 2: 3-chloro-4-methoxynitrobenzene With 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; water T=80°C; 3 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
反应条件
1,1-dimethylnitroethane; palladium diacetate in methanol T=25°C; 48 h;
参考文献
Joncour, Roxan; Susperregui, Nicolas; Pinaud, Noel; Miqueu, Karinne; Fouquet, Eric; Sotiropoulos, Jean-Marc; Felpin, Francois-Xavier
Chemistry - A European Journal, 2013 , vol. 19, # 28 p. 9291 - 9296
反应条件
1.1: 91 percent / diethyl ether / 12 h / Heating 2.1: tetrabutylammonium fluoride trihydrate / tetrahydrofuran; H2O / 1 h / 20 °C 2.2: 84 percent / 2-dicyclohexylphosphino-2',4',6'-triisopropylbiphenyl / [(η3-C3H5)PdCl]2 / tetrahydrofuran; H2O / 3 h / 80 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1715 - 1727
反应条件
1: aq. NaOH / ethanol 2: (i) KOH, EtOH, (ii) /BRN= 969135/ View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 6, p. 554 - 560
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Heating;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 7, # 7 p. 907 - 912
反应条件
1: NaOH-solution 2: glacial acetic acid; nitric acid View Scheme
参考文献
Chemische Berichte, , vol. 50, p. 600
反应条件
nitric acid; acetic acid
参考文献
Chemische Berichte, , vol. 50, p. 600
反应条件
1: potassium ferricyanide; diluted KOH-solution 2: dimethyl sulfate; methanol View Scheme
参考文献
Chemische Berichte, , vol. 50, p. 600
反应条件
1: NO<HSO4>, NaOAc View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 45, p. 1539 - 1542
反应条件
methanol; dimethyl sulfate
参考文献
Chemische Berichte, , vol. 50, p. 600
