3,5-双(苄氧基)-4-溴苯甲酸苄酯合成路线 （共 4 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=25°C; 4 h;
参考文献
Nicolaou; Bunnage; Bunnage, Mark E.; Koide; Koide, Kazunori
Journal of the American Chemical Society, 1994 , vol. 116, # 18 p. 8402 - 8403
Title/Abstract Full Text View citing articles Show Details
Nicolaou, K. C.; Koide, Kazunori; Bunnage, Mark E.
Chemistry--A European Journal, 1995 , vol. 1, # 7 p. 454 - 466
反应条件
1: 95 percent / NaOH / H2O / 12 h / 100 °C 2: 99 percent / CDI, DBU / dimethylformamide / 60 h / 40 °C View Scheme
参考文献
Lampe, John W.; Hughes, Philip F.; Biggers, Christopher K.; Smith, Shelley H.; Hu, Hong
Journal of Organic Chemistry, 1994 , vol. 59, # 18 p. 5147 - 5148
反应条件
sodium hydroxide in water T=100°C; 12 h;
参考文献
Lampe, John W.; Hughes, Philip F.; Biggers, Christopher K.; Smith, Shelley H.; Hu, Hong
Journal of Organic Chemistry, 1996 , vol. 61, # 14 p. 4572 - 4581
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; caesium carbonate in tetrahydrofuran; water
T=85 - 90°C; Suzuki-Miyaura vinylation; 48 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Brooker, Matthew D.; Cooper Jr., Stefan M.; Hodges, Dena R.; Carter, Rhiannon R.; Wyatt, Justin K.
Tetrahedron Letters, 2010 , vol. 51, # 51 p. 6748 - 6752
