5-溴-2,2’-联吡啶合成路线 (共 17 条)
反应条件
methanol; bromine in acetonitrile 4 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 36, # 23 p. 4077 - 4080
反应条件
2,2'-azo-bisisobutyronitrile; trichloromonobromomethane; Fonderma T=100°C; 20 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 36, # 36 p. 6471 - 6474
反应条件
1: n-butyllithium / diethyl ether 2: tetrakis(triphenylphosphine) palladium(0) / anhydrous xylene View Scheme
参考文献
Dalton Transactions, , vol. 42, # 6 p. 2062 - 2074
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 94, # 1-4 p. 405 - 410
反应条件
bromine electrophilic substitution on tris(2-pyridyl)phosphine; Product distribution;
参考文献
Phosphorus, Sulfur and Silicon and Related Elements, , vol. 109, # 1-4 p. 605 - 608
反应条件
N,N,N',N,-tetramethylethylenediamine; 1,5-bis-(diphenylphosphino)-pentane; Neutral lead acetate in 1,3,5-trimethyl-benzene 16 h; Heating;
参考文献
Veauthier, Jacqueline M.; Carlson, Christin N.; Collis, Gavin E.; Kiplinger, Jaqueline L.; John, Kevin D.
Synthesis, 2005 , # 16 art. no. M01305SS, p. 2683 - 2686
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in N,N-dimethyl-formamide T=100°C; Suzuki cross-coupling; 8 h;
参考文献
Vrabel, Milan; Hocek, Michal; Havran, Ludek; Fojta, Miroslav; Votruba, Ivan; Klepetarova, Blanka; Pohl, Radek; Rulisek, Lubomir; Zendlova, Lucie; Hobza, Pavel; Shih, I.-Hung; Mabery, Eric; Mackman, Richard
European Journal of Inorganic Chemistry, 2007 , # 12 p. 1752 - 1769