N-(3-氧代丙基)苯甲酰胺合成路线 (共 3 条)
反应条件
dicobalt octacarbonyl; hydrogen in toluene T=80°C; P=62324.2 Torr; 6 h;
参考文献
Laitar, David S.; Kramer, John W.; Whiting, Bryan T.; Lobkovsky, Emil B.; Coates, Geoffrey W.
Chemical Communications, 2009 , # 38 p. 5704 - 5706
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine 1.) CH2Cl2, -78 deg C; Multistep reaction;
参考文献
MaGee, David I.; Ramaseshan, Mahesh; Leach, James D.
Canadian Journal of Chemistry, 1995 , vol. 73, # 12 p. 2111 - 2118
反应条件
1: 1.67 g / triethylamine / CH2Cl2 / 16 h / 25 °C 2: 610 mg / 10percent aq. HCl / acetone / 16 h / 25 °C View Scheme
参考文献
Chan, Samantha; Braish, Tamim F.
Tetrahedron, 1994 , vol. 50, # 33 p. 9943 - 9950