反应条件
1.1: n-butyllithium; N,N'-dimethyl-N,N'-propyleneurea / tetrahydrofuran; hexane / 2 h / -78 °C / |Inert atmosphere
1.2: 3.5 h / -78 - -30 °C / |Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 0 °C
3.1: [PdCl2(1,3-bis(diphenylphosphino)propane)]; lithium triethylborohydride / tetrahydrofuran / 2 h / 0 °C / |Inert atmosphere
View Scheme
参考文献
Liu, Feng; Vijayakrishnan, Balakumar; Faridmoayer, Amirreza; Taylor, Thomas A.; Parsons, Thomas B.; Bernardes, Goncalo J.L.; Kowarik, Michael; Davis, Benjamin G.
Journal of the American Chemical Society, 2014 , vol. 136, # 2 p. 566 - 569
