反应条件
1: 1.) D2O, NaOD, 2.) D2SO4 / 1.) reflux, 6 h, 2.) reflux, 4.5 h
2: 90.8 percent / LiAlD4 / diethyl ether / 8 h / Heating
3: 85.1 percent / red phosphorous, Br2 / 85 - 90 °C
View Scheme
参考文献
Lipinski, K.; Lipinska, T.; Suszko-Purzycka, A.; Rykowski, A.
Polish Journal of Chemistry, 1993 , vol. 67, # 4 p. 667 - 672
