二(甲烷磺酸)1,3-丙二醇酯合成路线 （共 5 条）
反应条件
triethylamine in dichloromethane T=0 - 20°C; 2 h; Inert atmosphere;
参考文献
Hanes, Robert E.; Ellingsworth, Edward C.; Griffin, Scott T.; Rogers, Robin D.; Bartsch, Richard A.
ARKIVOC (Gainesville, FL, United States), 2010 , vol. 2010, # 7 p. 217 - 237,21
反应条件
triethylamine in dichloromethane T=-10°C;
参考文献
Gu, Xiao-Hui; Zong, Rushi; Kula, Nora S.; Baldessarini, Ross J.; Neumeyer, John L.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 23 p. 3049 - 3053
反应条件
in dimethyl sulfoxide T=75°C; 16 h;
参考文献
Poldy, Jacqueline; Peakall, Rod; Barrow, Russell A.
Tetrahedron Letters, 2008 , vol. 49, # 15 p. 2446 - 2449
反应条件
1: 2-methoxy-phenol With caesium carbonate in acetonitrile
T=20°C; 3 h; Inert atmosphereReflux;
2: propane-1,3-diyl bis[methanesulfonate] in acetonitrile
24 h; Inert atmosphereReflux;
参考文献
Hanes, Robert E.; Ellingsworth, Edward C.; Griffin, Scott T.; Rogers, Robin D.; Bartsch, Richard A.
ARKIVOC (Gainesville, FL, United States), 2010 , vol. 2010, # 7 p. 217 - 237,21
反应条件
in acetonitrile
electrolysis;
参考文献
Voss, Juergen; Buelow, Christian Von; Drews, Torsten; Mischke, Peter
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 6 p. 519 - 526
