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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
Crispine A
合成路线
（共 31 条）
6275-29-2
N-(3,4-二甲氧基苯乙基)乙酰胺
→
反应条件
15889-93-7
Crispine A
反应条件
1: 82 percent / AlCl3 / nitrobenzene / 2.5 h / 35 °C 2: 93 percent / 1N HCl / 18 h / Heating 3: NaBH4 / methanol / Ambient temperature 4: xylene / 24 h / Heating 5: 91 percent / LiAlH4 / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Orito, Kazuhiko; Matsuzaki, Tsutomu; Suginome, Hiroshi; Rodrigo, Russel
Heterocycles, 1988 , vol. 27, # 10 p. 2403 - 2412
121089-95-0
→
反应条件
15889-93-7
Crispine A
反应条件
1: xylene / 24 h / Heating 2: 91 percent / LiAlH4 / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Orito, Kazuhiko; Matsuzaki, Tsutomu; Suginome, Hiroshi; Rodrigo, Russel
Heterocycles, 1988 , vol. 27, # 10 p. 2403 - 2412
55716-88-6
→
反应条件
15889-93-7
Crispine A
反应条件
1: anhydrous iron chloride; di-tert-butyl peroxide / 1,2-dichloro-2-methylpropane; tert-butyl alcohol / 5 h / 110 °C / Inert atmosphere 2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 40 °C / Inert atmosphere View Scheme
参考文献
Shirakawa, Eiji; Uchiyama, Nanase; Hayashi, Tamio
Journal of Organic Chemistry, 2011 , vol. 76, # 1 p. 25 - 34
170960-49-3
→
反应条件
15889-93-7
Crispine A
反应条件
1: hydrogenchloride / water / 24 h 2: sodium tetrahydroborate / methanol / 0 °C View Scheme
参考文献
Saha, Sanjay; Venkata Ramana Reddy, Ch.; Patro, Balaram
Tetrahedron Letters, 2011 , vol. 52, # 31 p. 4014 - 4016
93-17-4
(3,4-二甲氧苯基)乙腈
→
反应条件
15889-93-7
Crispine A
反应条件
1: toluene-4-sulfonic acid / toluene / 4 h / |Molecular sieve; |Reflux 2: lithium aluminium tetrahydride; triethyl amine hydrochloride / tetrahydrofuran / |Inert atmosphere; |Cooling with ice View Scheme
参考文献
Huang, Huawen; Ji, Xiaochen; Wu, Wanqing; Jiang, Huanfeng
Chemical Communications, 2013 , vol. 49, # 32 p. 3351 - 3353
120-14-9
3,4-二甲氧基苯甲醛
→
反应条件
15889-93-7
Crispine A
反应条件
1.1: acetic acid; ammonium acetate / 20 - 120 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / |Reflux 3.1: toluene / 20 h / 20 °C / |Reflux 4.1: trichlorophosphate / toluene / 4.5 h / 20 °C / |Reflux 4.2: 16 h / 0 - 20 °C View Scheme
参考文献
Crestey, Francois; Jensen, Anders A.; Borch, Morten; Andreasen, Jesper Tobias; Andersen, Jacob; Balle, Thomas; Kristensen, Jesper Langgaard
Journal of Medicinal Chemistry, 2013 , vol. 56, # 23 p. 9673 - 9682
4230-93-7
→
反应条件
15889-93-7
Crispine A
反应条件
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / |Reflux 2.1: toluene / 20 h / 20 °C / |Reflux 3.1: trichlorophosphate / toluene / 4.5 h / 20 °C / |Reflux 3.2: 16 h / 0 - 20 °C View Scheme
参考文献
Crestey, Francois; Jensen, Anders A.; Borch, Morten; Andreasen, Jesper Tobias; Andersen, Jacob; Balle, Thomas; Kristensen, Jesper Langgaard
Journal of Medicinal Chemistry, 2013 , vol. 56, # 23 p. 9673 - 9682
56014-48-3
→
反应条件
15889-93-7
Crispine A
反应条件
hydrogenchloride; trichlorophosphate 1.) 100 deg C, 2.5 min, 2.) 50 deg C, 20 h; Yield given. Multistep reaction;
参考文献
Lochead, Alistair W.; Proctor, George R.; Caton, Michael P. L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2477 - 2489
56997-73-0
→
反应条件
15889-93-7
Crispine A
反应条件
1: phosphoryl chloride 2: tin; water; hydrochloric acid / Reagens 4: Aethanol View Scheme
参考文献
Child; Pyman
Journal of the Chemical Society, 1931 , p. 36,47
87995-16-2
→
反应条件
15889-93-7
Crispine A
+
87995-15-1
反应条件
hydrogenchloride; silver tetrafluoroborate 1) benzene, 0.5 h, 50 deg C, 2) 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Schell, Fred M.; Smith, Anita M.
Tetrahedron Letters, 1983 , vol. 24, # 18 p. 1883 - 1884
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