(2S)-2-甲氧基-1-丙醇合成路线 (共 25 条)
反应条件
Cu(L-Asp)(1,2-bis(4-pyridyl)ethylene)0.5(H2O)0.5(MeOH)0.5 T=25°C;
参考文献
Chemical Communications, , # 11 p. 1287 - 1289
反应条件
0.5 Pt/Al2O3; dihydrogen peroxide T=59.84°C; P=3750.38 Torr; 2 h; Inert atmosphereAutoclave;
参考文献
Catalysis Today, , vol. 187, # 1 p. 168 - 172
反应条件
carbon monoxide; hydrogen; cobalt T=200°C; P=661957 Torr;
反应条件
H(+)-zeolite-X in benzene T=25°C; 0.5 h; further alcohols, thiols, aminoalcohols; further catalyst; Product distribution;
参考文献
Journal of Physical Organic Chemistry, , vol. 8, # 2 p. 121 - 126
反应条件
1: With dichloromethane; tungsten hexachloride in Chloroform-D T=100°C; 3 h; 2: With water in Chloroform-D T=-20°C;
参考文献
Dalton Transactions, , vol. 39, # 22 p. 5367 - 5376
反应条件
potassium carbonate T=140°C; 6 h; Supercritical conditionsGreen chemistry;
参考文献
, vol. 35, # 11 p. 654 - 656,3
反应条件
potassium carbonate T=100°C; 6 h; Supercritical conditionsGreen chemistry;
参考文献
Fan, Bin; Qu, Bo; Cai, Liang; Chen, Qingchuan; Wen, Yicun; Zhang, Rui
2011 , vol. 35, # 11 p. 654 - 656,3
反应条件
sodium hydroxide; sodium tetrahydroborate; Hg(NO3)2 1) water, THF, 4h; 2) ca. 0.5 h; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 46, # 3 p. 531 - 538
反应条件
lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 10 min, 2.) Et2O, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1807 - 1810
参考文献
Journal of the American Chemical Society, , vol. 77, p. 2420,2423