反应条件
1.1: B-chloro-diisopinocampheylborane / dichloromethane / -5 - 0 °C 2.1: cerium(III) chloride / tetrahydrofuran / 0 - 5 °C 3.1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 0 - 5 °C 4.1: toluene-4-sulfonic acid / dichloromethane / 25 - 30 °C 5.1: water; sodium hydroxide / tetrahydrofuran; methanol / 25 - 30 °C 6.1: hydrogenchloride / water; ethyl acetate / 25 - 30 °C 7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 25 - 30 °C 7.2: 1 h / 0 - 5 °C 8.1: sodium methylate / methanol; N,N-dimethyl-formamide / 0 - 5 °C 9.1: ethyl acetate / 25 - 30 °C 10.1: sulfuric acid; water / 5 - 10 °C View Scheme
参考文献
Asian Journal of Chemistry, , vol. 23, # 10 p. 4536 - 4546
