2-甲基-3,4-二氢-2H-1-萘酮合成路线 （共 89 条）
反应条件
water; hydrogen bromide T=120°C; 2 h;
参考文献
Tsuchida, Hiroyuki; Tamura, Mutsuko; Hasegawa, Eietsu
Journal of Organic Chemistry, 2009 , vol. 74, # 6 p. 2467 - 2475
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: With tert-butyloxycarbonyl-L-aspartic acid in tetrahydrofuran; hexane T=-78°C; 3 h;
参考文献
Mitsuhashi, Kaori; Ito, Rie; Arai, Takayoshi; Yanagisawa, Akira
Organic Letters, 2006 , vol. 8, # 8 p. 1721 - 1724
反应条件
t-BuP4 in tetrahydrofuran; hexane T=-78°C; 0.5 h;
参考文献
Solladie-Cavallo; Sedy; Salisova; Biba; Welch; Nafie; Freedman
Tetrahedron Asymmetry, 2001 , vol. 12, # 19 p. 2703 - 2707
反应条件
potassium hydroxide; pentacarbonyliron(0) in ethanol; water 3 h; Heating;
参考文献
Johnson, Graham P.; Marples, Brian A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3399 - 3406
反应条件
Ephedrine; hydrogen; palladium on activated charcoal in acetonitrile T=20°C; 3 h;
参考文献
Thorey, Claire; Bouquillon, Sandrine; Helimi, Abdellatif; Henin, Francoise; Muzart, Jacques
European Journal of Organic Chemistry, 2002 , # 13 p. 2151 - 2159
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=80°C;
参考文献
Boger, Dale L.; Mathvink, Robert J.
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1429 - 1443
反应条件
N,N-bis[(2S)-2-N-tosyl-N-Li-amino-3-Me-butyl]-4-tosylamide; methyllithium; lithium bromide in tetrahydrofuran; diethyl ether T=-78°C; 1 h;
参考文献
Coumbarides, Gregory S.; Eames, Jason; Scheuermann, J. Erik W.; Sibbons, Kevin F.; Suggate, Michael J.; Watkinson, Michael
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 5 p. 906 - 909
反应条件
(NH4)2S2O8; [{(η5-C5Me5)RhCl}2(μ-Cl)2] in water T=110°C; 12 h; Inert atmosphereSealed tube;
参考文献
Li, Yang; Xue, Dong; Lu, Wei; Wang, Chao; Liu, Zhao-Tie; Xiao, Jianliang
Organic Letters, 2014 , vol. 16, # 1 p. 66 - 69
反应条件
1: H2 / Pd/C / acetonitrile / 1.17 h / 20 °C 2: acetonitrile 3: acetonitrile View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 20 p. 6528 - 6532
反应条件
in toluene T=110°C; 2 h;
参考文献
Hickman, Derek N.; Hodgetts, Kevin J.; Mackman, Peter S.; Wallace, Timothy W.; Wardleworth, J. Michael
Tetrahedron, 1996 , vol. 52, # 6 p. 2235 - 2260
