2-甲基-3,4-二氢-2H-1-萘酮合成路线 (共 89 条)
反应条件
2,5,8,11-tetramethyl-2,5,8,11-tetraazadodecane; lithium diisopropyl amide in ethylene glycol dimethyl ether T=-23°C; Alkylation; 0.666667 h;
参考文献
Tetrahedron Letters, , vol. 40, # 46 p. 8129 - 8132
反应条件
bis(1,5-cyclooctadiene)nickel (0); It-Bu2 in 1,3,5-trimethyl-benzene T=130°C; 1 h; Inert atmosphere;
参考文献
Hoshimoto, Yoichi; Hayashi, Yukari; Suzuki, Haruka; Ohashi, Masato; Ogoshi, Sensuke
Angewandte Chemie - International Edition, 2012 , vol. 51, # 43 p. 10812 - 10815
Angew. Chem., 2012 , vol. 124, # 43 p. 10970 - 10973,4
反应条件
isourea dilithium salt in tetrahydrofuran T=-78°C;
参考文献
Coumbarides, Gregory S.; Eames, Jason; Suggate, Michael J.; Weerasooriya, Neluka
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 7 p. 641 - 652
参考文献
Bulletin de la Societe chimique de France, , vol. 2, p. 628 - 631
反应条件
water in N,N-dimethyl-formamide T=160°C;
参考文献
Synlett, , # 6 p. 929 - 933
反应条件
sodium hydroxide T=50 - 55°C; Erhitzen des Reaktionsprodukts unter Durchleiten von Wasserdampf;
参考文献
Journal of the American Chemical Society, , vol. 62, p. 1708,1711
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in acetic acid
参考文献
Israel Journal of Chemistry, , vol. 3, p. 1 - 11
反应条件
1: aluminium chloride 2: amalgamated zinc; hydrochloric acid 3: concentrated sulfuric acid View Scheme
参考文献
Chemische Berichte, , vol. 56, p. 630
反应条件
sodium hydride in tetrahydrofuran T=0 - 20°C; Inert atmosphere; Reagent/catalyst;
参考文献
Grenning, Alexander J.; Van Allen, Christie K.; Maji, Tapan; Lang, Simon B.; Tunge, Jon A.
Journal of Organic Chemistry, 2013 , vol. 78, # 14 p. 7281 - 7287
反应条件
hydrogen; Pd-BaSO4 in toluene 48 h;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 49, # 9 p. 757 - 771