2-甲基-3,4-二氢-2H-1-萘酮合成路线 (共 89 条)
反应条件
hydrogenchloride in water T=40°C; 4 h; Yield given;
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 9-10 p. 297 - 303
反应条件
in isopropyl alcohol 0.666667 h; Irradiation;
参考文献
Yoshioka, Michikazu; Saitoh, Masahiro; Arai, Hideaki; Ichikawa, Keiji; Hasegawa, Tadashi
Tetrahedron, 1987 , vol. 43, # 22 p. 5237 - 5244
反应条件
lithium hexamethyldisilazane T=-78 - 20°C;
参考文献
Ghosh, Ketaki; Karmakar, Raju; Mal, Dipakranjan
European Journal of Organic Chemistry, 2013 , # 19 p. 4037 - 4046
反应条件
lithium hexamethyldisilazane T=-78 - 20°C;
参考文献
Ghosh, Ketaki; Karmakar, Raju; Mal, Dipakranjan
European Journal of Organic Chemistry, 2013 , # 19 p. 4037 - 4046
反应条件
sodium amide anschliessendes Kochen mit Methyljodid;
参考文献
Journal of the American Chemical Society, , vol. 65, p. 1085,1088
反应条件
1.1: diethyl cyanophosphonate / dimethylformamide / 0.5 h / 0 °C 1.2: Et3N / dimethylformamide / 2 h / 0 °C 2.1: 41 percent / 1,4,8,11-tetraazacyclotetradecane based Ni(II) complex; tetraethylammonium tosylate / dimethylformamide / 60 °C / Electrolysis View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 11 p. 4586 - 4589
反应条件
1: 34 percent / 1.) n-BuLi, diisopropylamine / tetrahydrofuran / 0.42 h / -65 °C 2: 70 percent / 1.) 1.2 eq. LDA; 2.) 4 eq. t-BuLi / tetrahydrofuran / 0.25 h / -70 °C View Scheme
参考文献
Tetrahedron, , vol. 50, # 41 p. 11839 - 11852
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in diethyl ether
参考文献
Journal of the Chemical Society, Chemical Communications, , # 18 p. 1419 - 1420
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 1 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Crich, David; Yao, Quingwei
Journal of Organic Chemistry, 1996 , vol. 61, # 10 p. 3566 - 3570
反应条件
CD in acetonitrile T=0°C; 0.416667 h; Irradiationasymmetric induction, var. of catalyst, solvent, temp., other additives, without irradiation; Product distribution;
参考文献
Monatshefte fur Chemie, , vol. 128, # 11 p. 1181 - 1188