2-甲基-3,4-二氢-2H-1-萘酮合成路线 （共 89 条）
反应条件
1: 85 percent / sodium hydride / benzene; dimethylformamide / 3 h / Heating 2: propan-2-ol / 0.67 h / Irradiation View Scheme
参考文献
Tetrahedron, , vol. 43, # 22 p. 5237 - 5244
反应条件
1: allyl 2-methyl-1-oxo-1,2,3,4-tetrahydronaphthalene-2-carboxylate With (2,2'-bipyridine)nickel(II) dibromide; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide Electrolysis; 2: methyl iodide With potassium carbonate in N,N-dimethyl-formamide Further stages.;
参考文献
European Journal of Organic Chemistry, , # 14 p. 2257 - 2259
反应条件
1: allyl 2-methyl-1-oxo-1,2,3,4-tetrahydronaphthalene-2-carboxylate With [Ni(2,2'-bipyridine)3(2+)][BF4(1-)]2; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide Electrolysis; 2: methyl iodide With potassium carbonate in N,N-dimethyl-formamide Further stages.;
参考文献
European Journal of Organic Chemistry, , # 14 p. 2257 - 2259
反应条件
1: 6 N aq. KOH / ethanol / 2 h / Heating 2: polyphosphoric ester / CHCl3 / Ambient temperature View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 29, # 4 p. 477 - 480
反应条件
sodium methylate in 1,4-dioxane
参考文献
Chemische Berichte, , vol. 108, p. 203 - 207
反应条件
1: 1.) Br2 2.) triethylamine / 1.) ether, -60 deg C, 0.5 h then 0 deg C; 2.) ether, -20 deg C 3: 1.2 N HCl / H2O / 4 h / 40 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 9-10 p. 297 - 303
反应条件
2: 1.2 N HCl / H2O / 4 h / 40 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 9-10 p. 297 - 303
反应条件
1: (i) Py, (ii) CrO3, aq. H2SO4 2: NaOMe / dioxane View Scheme
参考文献
Chemische Berichte, , vol. 108, p. 203 - 207
反应条件
chromium(VI) oxide; acetic acid
参考文献
Journal of Organic Chemistry, , vol. 39, # 10 p. 1416 - 1420
参考文献
Journal of Organic Chemistry, , vol. 69, # 20 p. 6528 - 6532
