2-甲基-3,4-二氢-2H-1-萘酮合成路线 (共 89 条)
反应条件
hydrogen; palladium on activated charcoal in n-heptane P=3750.3 Torr; Product distribution; Further Variations:Solvents;
参考文献
Chemistry Letters, , vol. 35, # 7 p. 780 - 781
反应条件
1: 87 percent / tetrahydrofuran / 1.5 h / -10 °C 2: 94 percent / toluene / 2 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 52, # 6 p. 2235 - 2260
反应条件
1: potassium carbonate / dimethyl sulfoxide / 20 °C / |Schlenk technique; |Inert atmosphere 2: sodium hydride / tetrahydrofuran / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 14 p. 7281 - 7287
反应条件
1: 1.) LDA / 1.) THF, hexane, -40 deg C, 3 h, 2.) THF, hexane, -40 deg C, 18 h, then room t. 2: 84 percent / aq. 10percent H2SO4 / 18 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 50, # 9 p. 2849 - 2864
反应条件
1-methoxy-2-phenylprop-1-enolate in tetrahydrofuran T=-78°C; 1 h; other reagent; Product distribution;
参考文献
Helvetica Chimica Acta, , vol. 72, p. 1248 - 1252
参考文献
Chemische Berichte, , vol. 56, p. 630
参考文献
Chemische Berichte, , vol. 51, p. 1600
反应条件
bei der Wasserdampfdestillation;
参考文献
Journal of the Chemical Society, , p. 2576
参考文献
Journal of the Chemical Society, , p. 2576
反应条件
perchloric acid in tetrachloromethane 10 h;
参考文献
Buksha, Svitlana; Coumbarides, Gregory S.; Dingjan, Marco; Eames, Jason; Suggate, Michael J.; Weerasooriya, Neluka
Journal of Labelled Compounds and Radiopharmaceuticals, 2005 , vol. 48, # 5 p. 337 - 352