2-甲基-3,4-二氢-2H-1-萘酮合成路线 （共 89 条）
反应条件
toluene-4-sulfonic acid
参考文献
Coumbarides, Gregory S.; Eames, Jason; Weerasooriya, Neluka
Journal of Labelled Compounds and Radiopharmaceuticals, 2001 , vol. 44, # 12 p. 871 - 879
反应条件
1: α-methyltetralone With N,N,N',N',N'',N''-hexamethylphosphoric triamide; sodium hydride in tetrahydrofuran T=20°C; 1 h; Inert atmosphere; 2: 1,1-dibromomethane in tetrahydrofuran T=85°C; 22 h; Inert atmosphere;
参考文献
Tsuchida, Hiroyuki; Tamura, Mutsuko; Hasegawa, Eietsu
Journal of Organic Chemistry, 2009 , vol. 74, # 6 p. 2467 - 2475
反应条件
1: LiAlH4; diethyl ether / Erhitzen des Reaktionsprodukts mit KHSO4 unter 20 Torr 2: SeO2; xylene View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 248,254
反应条件
aluminium trichloride; benzeneseleninic anhydride in toluene 1.5 h; Heating;
参考文献
Yamakawa, Koji; Satoh, Tsuyoshi; Ohba, Nobuyuki; Sakaguchi, Reiji; Takita, Satoshi; Tamura, Nobuhiko
Tetrahedron, 1981 , vol. 37, p. 473 - 480
反应条件
benzeneseleninic anhydride; sodium hydride in toluene 3.5 h; Heating; Yield given. Yields of byproduct given;
参考文献
Yamakawa, Koji; Satoh, Tsuyoshi; Ohba, Nobuyuki; Sakaguchi, Reiji; Takita, Satoshi; Tamura, Nobuhiko
Tetrahedron, 1981 , vol. 37, p. 473 - 480
反应条件
carbon disulfide; bromine Kochen des Reaktionsprodukts mit N.N-Dimethyl-anilin;
参考文献
Reetz, Manfred T.; Stephan, Wilfried
Liebigs Annalen der Chemie, 1980 , # 4 p. 533 - 541
反应条件
Oxonereg;; NH4Br in dichloromethane
参考文献
Tetrahedron Letters, , vol. 53, # 2 p. 191 - 195
反应条件
Kochen des Reaktionsprodukts mit N.N-Dimethyl-anilin;
参考文献
Tishler; Fieser; Wendler
Journal of the American Chemical Society, 1940 , vol. 62, p. 2866,2868
反应条件
hydrogenchloride; sodium hydroxide in N-methyl-acetamide
参考文献
Smith Kline and French Laboratories Limited
Patent: US4755511 A1, 1988 ;
反应条件
(i) Ph3CNa, Et2O, (ii) /BRN= 506256/, (iii) KOH, EtOH; Multistep reaction;
参考文献
Harnik,M.
Israel Journal of Chemistry, 1965 , vol. 3, p. 1 - 11
