2-苯基-1-乙炔硼酸频那醇酯合成路线 （共 36 条）
反应条件
copper diacetate in various solvent(s) T=60°C; 6 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Nishihara, Yasushi; Okamoto, Masanori; Inoue, Yoshiaki; Miyazaki, Mikihiro; Miyasaka, Mitsuru; Takagi, Kentaro
Tetrahedron Letters, 2005 , vol. 46, # 50 p. 8661 - 8664
反应条件
1,3-dimethyl-imidazolidin-2-one; potassium carbonate; triphenylphosphine; copper(l) chloride
T=120°C; 12 h;
参考文献
Ogawa, Daisuke; Li, Jing; Suetsugu, Masato; Jiao, Jiao; Iwasaki, Masayuki; Nishihara, Yasushi
Tetrahedron Letters, 2013 , vol. 54, # 6 p. 518 - 521
反应条件
copper(l) chloride in DMI
T=120°C; 0.5 h; Inert atmosphere;
参考文献
Nishihara, Yasushi; Saito, Daisuke; Inoue, Eiji; Okada, Yoshiaki; Miyazaki, Mikihiro; Inoue, Yoshiaki; Takagi, Kentaro
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 306 - 308
反应条件
in 1,3,5-trimethyl-benzene
refluxing mesitylene, 48 h; 53percent the mixt. of regioisomers (>98:2);
参考文献
Browne, Duncan L.; Vivat, Jerome F.; Plant, Andrew; Gomez-Bengoa, Enrique; Harrity, Joseph P. A.
Journal of the American Chemical Society, 2009 , vol. 131, p. 7762 - 7769
反应条件
1,3-dimethyl-imidazolidin-2-one; potassium carbonate; triphenylphosphine; copper(l) chloride
T=120°C; 12 h;
参考文献
Ogawa, Daisuke; Li, Jing; Suetsugu, Masato; Jiao, Jiao; Iwasaki, Masayuki; Nishihara, Yasushi
Tetrahedron Letters, 2013 , vol. 54, # 6 p. 518 - 521
反应条件
1: in tetrahydrofuran
T=45°C; Cycloaddition; 16 h;
2: With ammonium cerium(IV) nitrate; water; nitric acid in diethyl ether
Oxidation;
参考文献
Davies; Johnson; Harrity
Journal of Organic Chemistry, 2001 , vol. 66, # 10 p. 3525 - 3532
反应条件
1,3-dimethyl-imidazolidin-2-one; potassium carbonate; triphenylphosphine; copper(l) chloride
T=120°C; 12 h;
参考文献
Ogawa, Daisuke; Li, Jing; Suetsugu, Masato; Jiao, Jiao; Iwasaki, Masayuki; Nishihara, Yasushi
Tetrahedron Letters, 2013 , vol. 54, # 6 p. 518 - 521
反应条件
copper(l) chloride in DMI
T=120°C; 0.5 h; Inert atmosphere;
参考文献
Nishihara, Yasushi; Saito, Daisuke; Inoue, Eiji; Okada, Yoshiaki; Miyazaki, Mikihiro; Inoue, Yoshiaki; Takagi, Kentaro
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 306 - 308
反应条件
1,3-dimethyl-imidazolidin-2-one; potassium carbonate; triphenylphosphine; copper(l) chloride
T=120°C; 12 h;
参考文献
Ogawa, Daisuke; Li, Jing; Suetsugu, Masato; Jiao, Jiao; Iwasaki, Masayuki; Nishihara, Yasushi
Tetrahedron Letters, 2013 , vol. 54, # 6 p. 518 - 521
反应条件
1,3-dimethyl-imidazolidin-2-one; potassium carbonate; triphenylphosphine; copper(l) chloride
T=120°C; 12 h;
参考文献
Ogawa, Daisuke; Li, Jing; Suetsugu, Masato; Jiao, Jiao; Iwasaki, Masayuki; Nishihara, Yasushi
Tetrahedron Letters, 2013 , vol. 54, # 6 p. 518 - 521
