(S)-(-)-1-萘基-1-乙醇合成路线 （共 81 条）
反应条件
lipase B from Candida antarctica in cyclohexane T=50°C; 1.75 h; Resolution of racemate; optical yield given as percent ee;
参考文献
Li, Xiang; Shi, Yi; Wang, Zhoujun; Zhang, Yahong; Tang, Yi
Journal of Catalysis, 2012 , vol. 288, p. 24 - 32
反应条件
iodosylbenzene; iron(III) meso-tetraphenylporhinato chloride in dichloromethane T=0°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 55, # 11 p. 3628 - 3634
反应条件
triethylamine; planar-chiral DMAP derivative in 1,1-dimethylpropan-1-ol T=0°C; Acetylation;
参考文献
Journal of Organic Chemistry, , vol. 63, # 9 p. 2794 - 2795
反应条件
(2S,3R)-3-isopropyl-2-phenyl-3,4-dihydro-2H-pyrimido[2,1-b]benzothiazole; N-ethyl-N,N-diisopropylamine in chloroform T=20 - 25°C; 28 h; optical yield given as percent eeenantioselective reaction;
参考文献
Belmessieri, Dorine; Joannesse, Caroline; Woods, Philip A.; MacGregor, Callum; Jones, Caroline; Campbell, Craig D.; Johnston, Craig P.; Duguet, Nicolas; Concellon, Carmen; Bragg, Ryan A.; Smith, Andrew D.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 559 - 570
反应条件
4 A molecular sieve; Lipase from Burkholderia cepacia in 1,4-dioxane T=30°C; 48 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 35 p. 12228 - 12229
反应条件
4 A molecular sieve; subtilisin Carlsberg in 1,4-dioxane T=30°C; 48 h; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 127, # 35 p. 12228 - 12229
反应条件
1: methylmagnesium bromide With titanium(IV) isopropylate; bis[2-(N,N-dimethylamino)ethyl] ether; (S)-(minus;)-1,1'-bi-2-naphthol in tetrahydrofuran; tert-butyl methyl ether T=20°C; Inert atmosphereCooling with ice; 2: 1-naphthaldehyde in tetrahydrofuran; tert-butyl methyl ether T=20°C; Inert atmosphereCooling with ice; optical yield given as percent eeenantioselective reaction;
参考文献
Organic Letters, , vol. 11, # 24 p. 5578 - 5581
反应条件
vinyl acetate; Lipase PS in octane T=30°C; 8 h; Yields of byproduct given;
参考文献
Kato; Katayama; Gautam; Fujii; Kimoto
Bioscience, Biotechnology and Biochemistry, 1995 , vol. 59, # 2 p. 271 - 276
反应条件
endo-8,8-dimethyl-2-phenylphosphabicyclo[3.3.0]-octane in toluene T=-25°C; Activation energyProduct distribution; Further Variations:ReagentsTemperatures;
参考文献
Journal of Organic Chemistry, , vol. 68, # 13 p. 5020 - 5027
反应条件
(2S,3R)-3-isopropyl-2-phenyl-3,4-dihydro-2H-pyrimido[2,1-b]benzothiazole; N-ethyl-N,N-diisopropylamine in toluene T=-40°C; 1 h; optical yield given as percent eeenantioselective reaction;
参考文献
Belmessieri, Dorine; Joannesse, Caroline; Woods, Philip A.; MacGregor, Callum; Jones, Caroline; Campbell, Craig D.; Johnston, Craig P.; Duguet, Nicolas; Concellon, Carmen; Bragg, Ryan A.; Smith, Andrew D.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 559 - 570
