(S)-(-)-1-萘基-1-乙醇合成路线 （共 81 条）
反应条件
chiral phosphine acylation catalyst; polystyrene-bound mesitoate
参考文献
Journal of the American Chemical Society, , vol. 123, # 10 p. 2428 - 2429
反应条件
1: methyl 1-naphthyl ketone With aluminum oxide; sodium tetrahydroborate in hexane T=40°C; 3 h; 2: 2-acetyloxy-1-propene With Lipase 'Amano' PS-C II in hexane T=25°C; 12 h;
参考文献
Kamal, Ahmed; Sandbhor, Mahendra; Ramana
Tetrahedron Asymmetry, 2002 , vol. 13, # 8 p. 815 - 820
反应条件
(S)-(4-tert-butyl-2-thioxothiazolidin-3-yl)[4-(dimethylamino)pyridin-3-yl]methanone; triethylamine T=20°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2239 - 2242
反应条件
1,3-bis-[(R)-1-(1-naphthyl)ethyl]-4,5-dihydro-3H-imidazolium tetrafluoroborate; potassium tert-butylate in tetrahydrofuran T=-78 - -40°C; 4.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Organic Letters, , vol. 7, # 7 p. 1347 - 1349
反应条件
1: acetyl chloride With 1,4-diaza-bicyclo[2.2.2]octane; (S)-3,3'-bis-(2,4,6-triisopropylphenyl)-BINOL phosphoric acid in diethyl ether T=20°C; 0.0833333 h; Inert atmosphereResolution of racemate; 2: 1-(1-hydroxyethyl)naphthalene in diethyl ether T=-20°C; 5 h; Resolution of racemateInert atmosphere; optical yield given as percent ee;
参考文献
Organic Letters, , vol. 14, # 13 p. 3486 - 3489
反应条件
triethylamine; (-)-diethyl[3-(2-phenylnaphthyl)(4-pyridyl)]amine in toluene T=-78°C; 9 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 68, # 19 p. 7379 - 7385
反应条件
triethylamine; (-)-Diethyl[2-methyl-5-(2-phenyl-1-naphthyl)-4-pyridyl]amine in toluene T=-78°C; 9 h; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 15 p. 1785 - 1794
反应条件
C9H21ClO3Ti*C9H18O2 in tetrahydrofuran Yield given. Yields of byproduct given;
参考文献
Helvetica Chimica Acta, , vol. 70, p. 954 - 974
反应条件
triethylamine; (-)-diethyl[3-(2-phenylnaphthyl)(4-pyridyl)]amine in toluene T=-78°C; 9 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 68, # 19 p. 7379 - 7385
反应条件
triethylamine; (-)-diethyl[3-(2-phenylnaphthyl)(4-pyridyl)]amine in toluene T=-78°C; 9 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 68, # 19 p. 7379 - 7385
