(S)-(-)-1-萘基-1-乙醇合成路线 （共 81 条）
反应条件
potassium fluoride; C46H34Br4O6 in dichloromethane T=20°C; 120 h; optical yield given as percent eeenantioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 47 p. 8915 - 8917
反应条件
(5aS,10bR)-5a,10b-dihydro-2-(pentafluorophenyl)-4H,6H-indeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazinium tetrafluoroborate; 3-benzylriboflavin tetraacetate; triethylamine in toluene T=20°C; 4 h; Resolution of racemateAirMolecular sieve; optical yield given as percent eeenantioselective reaction;
参考文献
Chemistry - A European Journal, , vol. 17, # 29 p. 8009 - 8013
反应条件
Candida antarctica lipase B in n-heptane T=60°C; 3 h; Microwave irradiationResolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 81, p. 58 - 65
反应条件
Candida antarctica lipase B in n-heptane T=60°C; 3 h; Microwave irradiationResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 81, p. 58 - 65
反应条件
{3-[2-(3,5-dimethylphenyl)naphthalen-1-yl]pyridin-4-yl}diethylamine; triethylamine in toluene T=-78°C; 2 h; optical yield given as percent ee;
参考文献
Journal of the American Chemical Society, , vol. 134, # 22 p. 9390 - 9399
反应条件
lipase from candida antartica in aq. phosphate buffer T=30°C; 48 h;
参考文献
Letters in Organic Chemistry, , vol. 9, # 9 p. 615 - 621
反应条件
lipase from candida antartica in aq. phosphate buffer T=30°C; 48 h;
参考文献
Letters in Organic Chemistry, , vol. 9, # 9 p. 615 - 621
反应条件
(S)-N-(1-(tert-butylcarbamoyl)-1-(4-(dimethylamino)pyridin-3-yl)methyl)-L-valinemethyl ester; triethylamine in toluene T=-78°C; 15 h; enantioselective reaction;
参考文献
Heterocycles, , vol. 87, # 2 p. 329 - 340
反应条件
Na-Pi buffer in acetone 48 h; tubers of Helianthus tuberosus presence, pH 5.9; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Phytochemistry, , vol. 47, # 8 p. 1531 - 1534
反应条件
1: lipase from candida antartica / aq. phosphate buffer / 48 h / 30 °C 2: sodium hydroxide; water / 2 h / 20 °C View Scheme
参考文献
Letters in Organic Chemistry, , vol. 9, # 9 p. 615 - 621
