(S)-(-)-1-萘基-1-乙醇合成路线 （共 81 条）
反应条件
1: lipase from candida antartica / aq. phosphate buffer / 48 h / 30 °C 2: sodium hydroxide; water / 2 h / 20 °C View Scheme
参考文献
Letters in Organic Chemistry, , vol. 9, # 9 p. 615 - 621
反应条件
water; sodium hydroxide T=20°C; 2 h;
参考文献
Letters in Organic Chemistry, , vol. 9, # 9 p. 615 - 621
反应条件
water; sodium hydroxide T=20°C; 2 h;
参考文献
Letters in Organic Chemistry, , vol. 9, # 9 p. 615 - 621
反应条件
Pseudomonas cepacia lipase in 1,1,1,2-tetrafluoroethane 24 h; Resolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Tetrahedron Letters, , vol. 50, # 26 p. 3543 - 3546
反应条件
methanol; sodium hydroxide T=20°C; Inert atmosphereHeating; optical yield given as percent ee;
参考文献
Journal of Organic Chemistry, , vol. 75, # 14 p. 4674 - 4685
反应条件
methanol; sodium hydroxide T=20°C; Inert atmosphereHeating; optical yield given as percent ee;
参考文献
Journal of Organic Chemistry, , vol. 75, # 14 p. 4674 - 4685
反应条件
1: triethylamine; 4-(N,N-dimethlyamino)pyridine / diethyl ether 2: Candida antarctica lipase fraction B immobilized on acrylic resin / aq. phosphate buffer; diethyl ether / 48 h / 20 °C / pH 7 / |Resolution of racemate; |Enzymatic reaction View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 24, # 5-6 p. 290 - 296
反应条件
C22H29N3O3; triethylamine; C16H23P*BF4(1-)*H(1+) in toluene T=-40°C; 3 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 75, # 14 p. 4674 - 4685
反应条件
1,1-dimethylpropan-1-ol; (P,S)-13-bromo-4-ethyl-2,6-dimethyl-3-phenyl-5,6-dihydro-2H-naphtho[2',1':3,4]isochromeno[6,5-c][1,6]naphthyridine; triethylamine T=0°C;
参考文献
Chemical Communications, , vol. 48, # 91 p. 11181 - 11183
反应条件
1: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 20 °C / |Inert atmosphere 2: lipase from candida antartica / aq. phosphate buffer / 48 h / 30 °C View Scheme
参考文献
Letters in Organic Chemistry, , vol. 9, # 9 p. 615 - 621
