Alpha,Alpha,Alpha,Alpha-四溴对二甲苯合成路线 （共 11 条）
反应条件
bromine T=130 - 160°C; 5 h;
参考文献
Grechkina, E. V.; Sochilin, V. A.; Pebalk, A. V.; Kardash, I. E.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 10 p. 1663 - 1665
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 10 p. 1999 - 2001
反应条件
hydrogen bromide; sodium bromide in chloroform; water T=5 - 15°C; Electrolysis;
参考文献
Kulangiappar; Karthik; Kulandainathan, M. Anbu
Synthetic Communications, 2009 , vol. 39, # 13 p. 2304 - 2309
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 141, p. 44,57
反应条件
thionyl bromide Heating; Yield given;
参考文献
Synthetic Communications, , vol. 13, # 1 p. 7 - 14
反应条件
SbF3 T=120°C; P=40 Torr;
参考文献
Grechkina, E. V.; Sochilin, V. A.; Pebalk, A. V.; Kardash, I. E.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 10 p. 1663 - 1665
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 10 p. 1999 - 2001
反应条件
1: 85 percent / SbF3 / 120 °C / 40 Torr 2: 55 percent / N-bromosuccinimide / CCl4 / Heating; Irradiation 3: Cu / 640 °C 4: toluene / 110 °C View Scheme
参考文献
Grechkina, E. V.; Sochilin, V. A.; Pebalk, A. V.; Kardash, I. E.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 10 p. 1663 - 1665
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 10 p. 1999 - 2001
反应条件
1: 85 percent / SbF3 / 120 °C / 40 Torr 2: 55 percent / N-bromosuccinimide / CCl4 / Heating; Irradiation View Scheme
参考文献
Grechkina, E. V.; Sochilin, V. A.; Pebalk, A. V.; Kardash, I. E.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 10 p. 1663 - 1665
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 10 p. 1999 - 2001
反应条件
sulfuric acid T=120 - 130°C;
参考文献
Ruzicka; Buijs; Stoll
Helvetica Chimica Acta, 1932 , vol. 15, p. 1220,1224
Full Text Show Details
Weissberger; Bach
Chemische Berichte, 1932 , vol. 65, p. 24,28
Full Text Show Details
Deluchat
Annales de Chimie (Cachan, France), 1934 , vol. <11> 1, p. 181,186, 208
Full Text Show Details
Snell; Weissberger
Org. Synth. Coll., 1955 , vol. Vol. III, p. 788
参考文献
Thiele; Guenther
Justus Liebigs Annalen der Chemie, 1906 , vol. 347, p. 109
Full Text Show Details
Hoenig
Monatshefte fuer Chemie, 1888 , vol. 9, p. 1150
参考文献
Thiele; Guenther
Justus Liebigs Annalen der Chemie, 1906 , vol. 347, p. 109
