pyridine; thionyl chloride; diethyl ether

1: potassium permanganate; acetone 2: diethyl ether; thionyl chloride; pyridine View Scheme

1: aqueous KOH / 110 - 120 °C 2: potassium permanganate; acetone 3: diethyl ether; thionyl chloride; pyridine View Scheme

1: aqueous KOH / 110 - 120 °C 2: potassium permanganate; acetone 3: diethyl ether; thionyl chloride; pyridine View Scheme

暂无反应条件数据

1: 1.) potassium benzoate, 2.) K2CO3 / 1.) 170/180 deg C, 8 h, 2.) acetone, reflux, 2.5-4 h 2: 86 percent / AlBr3 / acetonitrile / 0.33 h / 0 - 5 °C 3: 89 percent / K2CO3 / acetone / Heating 4: 89 percent / AlBr3 / acetonitrile / 1 h / Ambient temperature 5: 95 percent / K2CO3 / methanol / 2 h / Heating 6: 89 percent / H2 / 10percent palladium on charcoal / ethyl acetate; methanol View Scheme