N-羟基-4-甲基苯磺酰胺合成路线 （共 6 条）
反应条件
hydroxylamine hydrochloride; magnesium oxide in methanol; water T=20°C; 2 h; chemoselective reaction;
参考文献
Sirsalmath, Kiran; Suarez, Sebastian A.; Bikiel, Damian E.; Doctorovich, Fabio
Journal of Inorganic Biochemistry, 2013 , vol. 118, p. 134 - 139
反应条件
sodium tetrahydroborate in 1,4-dioxane T=5 - 10°C; 0.666667 h;
参考文献
Oae, Shigeru; Shinhama, Koichi; Fujimori, Ken; Kim, Yong Hae
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 3 p. 775 - 784
反应条件
1: 54 percent / N2O4 / CCl4; diethyl ether / 0.17 h / 0 °C 2: 16 percent / NaBH4 / dioxane / 0.67 h / 5 - 10 °C View Scheme
参考文献
Oae, Shigeru; Shinhama, Koichi; Fujimori, Ken; Kim, Yong Hae
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 3 p. 775 - 784
参考文献
v.Meyer,E.
Journal fuer Praktische Chemie (Leipzig), 1901 , vol. <2>63, p. 176
Chem. Zentralbl., 1901 , vol. 72, # I p. 455
反应条件
1: Et3N
2: Et3N / Heating
View Scheme
参考文献
Okahara,M.; Swern,D.
Tetrahedron Letters, 1969 , p. 3301 - 3304
反应条件
dihydrogen peroxide in water
24 h; Ambient temperature;
参考文献
Briganti; Pierattelli; Scozzafava; Supuran
European Journal of Medicinal Chemistry, 1996 , vol. 31, # 12 p. 1001 - 1010
