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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1595-09-1
合成路线
（共 15 条）
29540-83-8
对苄基三氟甲磺酸
+
72665-98-6
→
反应条件
1595-09-1
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tetra-(n-butyl)ammonium iodide; bis(dibenzylideneacetone) palladium in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=60°C; 4 h;
参考文献
Piber, Michael; Jensen, Anne Eeg; Rottlaender, Mario; Knochel, Paul
Organic Letters, 1999 , vol. 1, # 9 p. 1323 - 1326
628-17-1
1-碘戊烷
+
4294-57-9
对甲苯基溴化镁
→
反应条件
1595-09-1
反应条件
1: (4-Methylphenyl)-magnesium bromide With zinc(II) chloride in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 2: With methyl-magnesium chloride in tetrahydrofuran T=-20°C; 0.25 h; Inert atmosphere; 3: n-amyl iodide With triphenylphosphine; nickel dichloride in tetrahydrofuran T=0 - 20°C; 1 h; Inert atmosphere; regioselective reaction;
参考文献
Pekel, Oezgen Oemuer; Erdik, Ender
Tetrahedron Letters, 2011 , vol. 52, # 52 p. 7087 - 7090
543-59-9
1-氯戊烷
+
4294-57-9
对甲苯基溴化镁
→
反应条件
1595-09-1
反应条件
p-tert-butyl-p-(2',6'-dimethoxy-biphenyl-2-yl)phosphine chloride; palladium diacetate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=25°C; Kumada-Corriu coupling; 20.4667 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Kapdi, Anant R.; Schulzke, Carola
Organic Letters, 2010 , vol. 12, # 10 p. 2298 - 2301
122-56-5
三正丁基硼
+
40739-81-9
→
反应条件
1595-09-1
反应条件
tetra(n-butyl)ammonium hydroxide in tetrahydrofuran; methanol 1 h; Heating;
参考文献
Kabalka, George W.; Maddox, John T.; Bogas, Ekaterini; Kelley, Shane W.
Journal of Organic Chemistry, 1997 , vol. 62, # 11 p. 3688 - 3695
122-56-5
三正丁基硼
+
189328-39-0
→
反应条件
1595-09-1
反应条件
tetra(n-butyl)ammonium hydroxide in tetrahydrofuran; methanol 1 h; Heating;
参考文献
Kabalka, George W.; Maddox, John T.; Bogas, Ekaterini; Kelley, Shane W.
Journal of Organic Chemistry, 1997 , vol. 62, # 11 p. 3688 - 3695
104-87-0
对甲基苯甲醛
→
反应条件
1595-09-1
反应条件
1: 29 percent / Ph3P / Pd(acac)2 / dioxane / 72 h / Heating 2: H2 / Pd-C / ethyl acetate View Scheme
参考文献
Kabalka, George W.; Maddox, John T.; Bogas, Ekaterini; Kelley, Shane W.
Journal of Organic Chemistry, 1997 , vol. 62, # 11 p. 3688 - 3695
628-71-7
1-庚炔
+
78-79-5
异戊二烯
→
反应条件
1595-09-1
+
113768-26-6
+
113768-39-1
+
113768-31-3
反应条件
[Rh(1,5-cyclooctadiene)(1,4-bis(diphenylphosphino)butane)]PF6 in dichloromethane T=25°C; 145 h; in a sealed tube under argon atmosphere; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Matsuda, Isamu; Shibata, Masahiro; Sato, Susumu; Izumi, Yusuke
Tetrahedron Letters, 1987 , vol. 28, # 29 p. 3361 - 3362
53496-99-4
→
反应条件
1595-09-1
反应条件
nickel Hydrogenation;
参考文献
Phillips Petr. Co.
Patent: US2471922 , 1944 ;
Full Text Show Details
Phillips Petr. Co.
Patent: US2430661 , 1944 ;
Full Text Show Details
Phillips Petr. Co.
Patent: US2404120 , 1944 ;
Full Text Show Details
Phillips Petr. Co.
Patent: US2430660 , 1944 ;
6853-58-3
+
60484-66-4
→
反应条件
1595-09-1
反应条件
magnesium in diethyl ether 5 h; Ambient temperature; Yield given;
参考文献
Cereghetti, Marco; Marbet, Roman; Schleich, Kuno
Helvetica Chimica Acta, 1982 , vol. 65, # 4 p. 1318 - 1330
122-56-5
三正丁基硼
+
40739-81-9
→
反应条件
1595-09-1
+
91763-35-8
反应条件
sodium perborate; 1,8-diazabicyclo[5.4.0]undec-7-ene 1.) THF, reflux, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kabalka, George W.; Maddox, John T.; Bogas, Ekaterini; Kelley, Shane W.
Journal of Organic Chemistry, 1997 , vol. 62, # 11 p. 3688 - 3695
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