3-甲苯磺酰-6-噁-双环[3.1.0]己烷合成路线 （共 4 条）
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=20°C; 4 h;
参考文献
Unthank, Matthew G.; Hussain, Nigel; Aggarwal, Varinder K.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 42 p. 7066 - 7069
反应条件
Oxonereg;; 1,1,1-trifluoropropanone; sodium hydrogencarbonate; (ethylenedinitrilo)tetraacetic acid disodium salt in water; acetonitrile T=0°C;
参考文献
Hodgson, David M.; Miles, Timothy J.; Witherington, Jason
Tetrahedron, 2003 , vol. 59, # 49 p. 9729 - 9742
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane; isopropyl alcohol
参考文献
Bayer Aktiengesellschaft
Patent: US6133260 A1, 2000 ;
反应条件
1.1: O3 / CH2Cl2; methanol / -78 °C 1.2: 96 percent / Zn; acetic acid / CH2Cl2; methanol / 21 h / -78 - 20 °C 2.1: 81 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 4 h / 20 °C View Scheme
参考文献
Unthank, Matthew G.; Hussain, Nigel; Aggarwal, Varinder K.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 42 p. 7066 - 7069
