[1-(叔丁基二甲基硅烷基)-1H-3-吲哚基]硼酸合成路线 （共 4 条）
反应条件
1: With tert.-butyl lithium in tetrahydrofuran 2: With boric acid trimethyl ester in tetrahydrofuran
参考文献
Kawasaki, Ikuo; Katsuma, Hideo; Nakayama, Yohko; Yamashita, Masayuki; Ohta, Shunsaku
Heterocycles, 1998 , vol. 48, # 9 p. 1887 - 1901
反应条件
1.1: NBS / tetrahydrofuran / 6 h / -78 °C 2.1: t-BuLi / tetrahydrofuran / 0.33 h / -78 °C 2.2: B(OEt)3 / tetrahydrofuran / 2 h View Scheme
参考文献
Yang, Cai-Guang; Liu, Gang; Jiang, Biao
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9392 - 9396
反应条件
1: Na2CO3 / Pd(PPh3)4 / dimethylformamide; H2O / 1 h / 150 °C
2: 66.9 mg / TBAF*3H2O / dimethylformamide; H2O / 0.17 h / 20 °C
View Scheme
参考文献
Fuerstner, Alois; Krause, Helga; Thiel, Oliver R
Tetrahedron, 2002 , vol. 58, # 32 p. 6373 - 6380
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in methanol; benzene
Suzuki-Miyaura coupling; 1 h; Heating;
参考文献
Nishida, Atsushi; Miyashita, Naoki; Fuwa, Mihoko; Nakagawa, Masako
Heterocycles, 2003 , vol. 59, # 2 p. 473 - 476
