hydrogenchloride

暂无反应条件数据

NaH2PO2*H2O in water (N2); std. Schlenk technique; mixt. of GeO2, NaH2PO2*H2O and HCl in H2O was refluxed at 99-102°C for 4 h under agitation; acrylic acid was added dropwise at -10 to -5°C for 2 h; stirred for 10 h while warmed to room temp.; extd. (Et2O); org. layer septd.; dried (MgSO4, 4 h); evapd. (vac.); recrystd. (CH2Cl2/ether);

O(SiH(CH3)2)2 in neat (no solvent) standing of the react. mixture at room temp. for about 5 days; distn.;

hydroquinone in neat (no solvent) mixt., contg. hydroquinone (polymerization inhibitor), kept 30 days at 20°C; pptn., liquid phase sepd. (decantation), crystals washed (cold hexane);

0 °C, work-up;