(2S)-N-Fmoc-6-叠氮基己酸合成路线 (共 4 条)
反应条件
imidazole-1-sulfonyl azide hydrochloride; CuSO4‵5H2O; potassium carbonate in methanol; water 5 h;
参考文献
Byrne, Cillian; McEwan, Paul A.; Emsley, Jonas; Fischer, Peter M.; Chan, Weng C.
Chemical Communications, 2011 , vol. 47, # 9 p. 2589 - 2591
反应条件
imidazole-1-sulfonyl azide hydrochloride; potassium carbonate; copper(II) sulfate in methanol; water T=20°C; pH=8.5;
参考文献
Mulder, Gwenn E.; Kruijtzer, John A. W.; Liskamp, Rob M. J.
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 80 p. 10007 - 10009,3
Title/Abstract Full Text Show Details
Mulder, Gwenn E.; Kruijtzer, John A. W.; Liskamp, Rob M. J.
Chemical Communications, 2012 , vol. 48, # 80 p. 10007 - 10009
反应条件
sodium hydroxide in 1,4-dioxane; water T=20°C; pH=8 - 9; 2.5 h;
参考文献
European Journal of Organic Chemistry, , # 31 p. 5308 - 5314
反应条件
sodium hydrogencarbonate; copper(II) sulfate in methanol; water T=20°C; pH=8 - 9;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 8 p. 1901 - 1904