2,2’,6,6’-四氯联苯合成路线 （共 14 条）
反应条件
copper T=230°C; 288 h;
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
反应条件
1: 1.) NaNO2, aq. H2SO4, 2.) KI / 1.) 0-5 deg C, 10 min, 2.) 0 deg C, 15 min; r.t., 1 h 2: 59 percent / Cu / 288 h / 230 °C View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 29, # 6 p. 679 - 685
反应条件
hydrogenchloride Diazotization.Behandlung der Diazoniumsalz-Loesung mit Aethanol;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 53, p. 359,362
反应条件
1: zinc; aq.-ethanolic NaOH-solution 2: zinc; acetic acid; ethanol 3: aqueous sulfuric acid 4: concentrated aqueous HCl / Diazotization.Behandlung der Diazoniumsalz-Loesung mit Aethanol View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 53, p. 359,362
反应条件
1: aqueous sulfuric acid 2: concentrated aqueous HCl / Diazotization.Behandlung der Diazoniumsalz-Loesung mit Aethanol View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 53, p. 359,362
反应条件
1: zinc; acetic acid; ethanol 2: aqueous sulfuric acid 3: concentrated aqueous HCl / Diazotization.Behandlung der Diazoniumsalz-Loesung mit Aethanol View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 53, p. 359,362
反应条件
aluminium trichloride; sulfuryl dichloride in dichloromethane 1 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
反应条件
aluminium trichloride; sulfuryl dichloride in dichloromethane 1 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
反应条件
aluminium trichloride; sulfuryl dichloride in dichloromethane 1 h; Ambient temperature; Product distribution;
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
反应条件
aluminium trichloride; sulfuryl dichloride in dichloromethane 1 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Waller, Stephen C.; Mash, Eugene A.
Organic Preparations and Procedures International, 1997 , vol. 29, # 6 p. 679 - 685
