反应条件
Multi-step reaction with 5 steps 1.1: 0.5 h / |Reflux; |Inert atmosphere1.2: 10 h / |Reflux; |Inert atmosphere2.1: methanol / 0.5 h / 20 °C / |Reflux; |Inert atmosphere2.2: |Reflux; |Inert atmosphere3.1: thionyl chloride / 4 h / |Reflux; |Inert atmosphere4.1: AlCl3, aluminium chloride / chloroform / 10 h / |Reflux; |Inert atmosphere5.1: AlCl3, aluminium chloride / toluene / 1 h / 20 °C / |Reflux; |Inert atmosphere
参考文献
Khan, Ashna A.; Kamena, Faustin; Timmer, Mattie S.M.; Stocker, Bridget L. Organic and Biomolecular Chemistry, 2013 , vol. 11, # 6 p. 881 - 885