3-环己基-3-氧代丙酸乙酯合成路线 （共 21 条）
反应条件
1: Na 2: 1) 0.2 N NaOH / 1. 20 h, room temp.; 2. pyrolysis at 110 deg C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 1 p. 43 - 47
反应条件
diethyl ether; sodium
参考文献
Chemische Berichte, , vol. 40, p. 3055
反应条件
chloro-trimethyl-silane; 1,8-diazabicyclo[5.4.0]undec-7-ene 1.) acetonitrile, room t.; 2.) 0 degC, 0.5 h, room t., 17 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 35, # 50 p. 9323 - 9326
反应条件
chloro-trimethyl-silane; 1,8-diazabicyclo[5.4.0]undec-7-ene 1.) acetonitrile, room t., 4 h; 2.) 0.5 h, room t., 5 h, 0 degC; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 35, # 50 p. 9323 - 9326
反应条件
Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 31, # 35 p. 4991 - 4994
反应条件
Et3N-5HF; 1-(iodo)-4-methylbenzene electrolysis: smooth Pt sheets as the anode and the cathode, undivided cell, 1.5 V (vs. Ag/Ag(+)), 10.0 F/mol;
参考文献
Hara, Shoji; Hatakeyama, Tsuyoshi; Chen, Sheng-Qi; Ishi-I, Kenji; Yoshida, Masanori; Sawaguchi, Masanori; Fukuhara, Tsuyoshi; Yoneda, Norihiko
Journal of Fluorine Chemistry, 1998 , vol. 87, # 2 p. 189 - 192
反应条件
1: 4-Acetylaminobenzenesulfonyl Azide; triethylamine / acetonitrile / 16 h / 0 - 20 °C / |Inert atmosphere; |Enzymatic reaction 2: HBF4*Et2O / dichloromethane / 5 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Pasceri, Raffaele; Bartrum, Hannah E.; Hayes, Christopher J.; Moody, Christopher J.
Chemical Communications, 2012 , vol. 48, # 99 p. 12077 - 12079
反应条件
sulfuric acid; potassium carbonate in dichloromethane; water; acetone; toluene; benzene
参考文献
U.S. Philips Corporation
Patent: US3996245 A1, 1976 ;
参考文献
American Cyanamid Company
Patent: US4029492 A1, 1977 ;
参考文献
Fray, M. Jonathan; Bull, David J.; Cooper, Kelvin; Parry, M. John; Stefaniak, Mark H.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 18 p. 3524 - 3535
