1,4-二(4-甲氧基苯基)-1,4-丁烷二酮合成路线 （共 34 条）
反应条件
1: NaH / paraffin; toluene / Heating
2: toluene-4-sulfinic acid <Li salt> / H2O; dimethylformamide / (electrolysis)
View Scheme
参考文献
Lamm,B.; Samuelsson,B.
Acta Chemica Scandinavica (1947-1973), 1970 , vol. 24, p. 561 - 568
反应条件
1: (i) AlCl3, 1,2-dichloro-ethane, (ii) Et3N, dioxane
2: Et3N, 5-(2-hydroxyethyl)-3,4-dimethylthiazolium iodide / dioxane
View Scheme
参考文献
Stetter,H.; Nienhaus,J.
Chemische Berichte, 1978 , vol. 111, p. 2825 - 2832
反应条件
aluminium trichloride; nitrobenzene
T=0°C;
参考文献
Winternitz; Mousseron
Bulletin de la Societe Chimique de France, 1948 , p. 1087,1090
反应条件
3,4-dimethyl-5-(2-hydroxyethyl)-thiazolium iodide; triethylamine in 1,4-dioxane
参考文献
Stetter,H.; Nienhaus,J.
Chemische Berichte, 1978 , vol. 111, p. 2825 - 2832
反应条件
in tetrahydrofuran
T=20°C; 24 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Crombie, Leslie; Hardy, Robert; Knight, David W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1373 - 1380
反应条件
in tetrahydrofuran
T=20°C; 24 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Crombie, Leslie; Hardy, Robert; Knight, David W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1373 - 1380
反应条件
(i) NaH, THF, (ii) /BRN= 743112/, KI, acetone, (iii) KOH; Multistep reaction;
参考文献
Lawson,J.E. et al.
Journal of Medicinal Chemistry, 1974 , vol. 17, p. 383 - 386
反应条件
methyloxirane in water; acetonitrile
4 h; Irradiation;
参考文献
Dhavale, Dilip D.; Mali, Vasant P.; Sudrik, Surendra G.; Sonawane, Harikisan R.
Tetrahedron, 1997 , vol. 53, # 49 p. 16789 - 16794
反应条件
in methanol
Ambient temperatureelectrolysis;
参考文献
Kojima, Masanobu; Sakuragi, Hirochika; Tokumaru, Katsumi
Chemistry Letters, 1981 , p. 1707 - 1710
反应条件
hydrogenchloride
1.) THF, 66 deg C, 2 h, 2.) THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rahman, M. T.; Nur, H. P.
Journal of the Indian Chemical Society, 1994 , vol. 71, # 6-8 p. 469 - 474
