1: 98 percent / KOH / ethanol / 2 h / Heating 2: 86 percent / diethyl ether / 0 - 20 °C View Scheme

1: 98 percent / KOH / ethanol / 2 h / Heating 2: 86 percent / diethyl ether / 0 - 20 °C 3: 80 percent / pyridine / 48 h / 2 - 20 °C 4: SOCl2 / 0.5 h / 65 - 70 °C 5: Br2 / SOCl2 / 5 h / 60 °C 6: 6.79 g / 2 h / Heating 7: CaCO3 / N,N-dimethyl-acetamide / 2 h / Heating 8: 2.47 g / aq. KOH / methanol / 10 h / Heating 9: 85 percent / CrO3; aq. H2SO4 / 1 h / 50 °C View Scheme

1: 98 percent / KOH / ethanol / 2 h / Heating 2: 86 percent / diethyl ether / 0 - 20 °C 3: 80 percent / pyridine / 48 h / 2 - 20 °C View Scheme

dicobalt octacarbonyl; carbon monoxide; hydrogen T=170°C; P=51714.8 Torr; 0.5 h;

ammonium nitrate in methanol T=20°C; 36 h;

1: ricinoleic acid methyl ester With sodium periodate in methanol 15 h; 2: methanol With toluene-4-sulfonic acid T=40°C; 1.5 h;

1: (Z)-9-octadecenoic acid With ozone in methanol; dichloromethane T=2°C; 2: With dimethylsulfide in methanol; dichloromethane T=20°C; 16 h; 3: methanol With toluene-4-sulfonic acid in dichloromethane T=20°C; 16 h;

1: 64 percent / O2 / methanol / 3.5 h / -65 °C 2: 64 percent / NH4NO3 / methanol / 36 h / 20 °C View Scheme

暂无反应条件数据

hydrogenchloride in methanol