S-Boc-4-甲氧基-β-苯丙氨酸合成路线 （共 5 条）
反应条件
sodium hydroxide in tetrahydrofuran 4 h; Ambient temperature;
参考文献
Matsuura, Fumiyoshi; Hamada, Yasumasa; Shioiri, Takayuki
Tetrahedron, 1994 , vol. 50, # 31 p. 9457 - 9470
反应条件
1: 94 percent / pyridine / 2 h / 0 °C 2: 83 percent / 18-crown-6 / dimethylsulfoxide / 3 h / 50 °C 3: 3.7 g / conc. HCl / tetrahydrofuran / 12 h / 100 °C 4: 4.75 percent / 1N NaOH / tetrahydrofuran / 4 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 50, # 31 p. 9457 - 9470
反应条件
1: 3.7 g / conc. HCl / tetrahydrofuran / 12 h / 100 °C 2: 4.75 percent / 1N NaOH / tetrahydrofuran / 4 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 50, # 31 p. 9457 - 9470
反应条件
1: LiCl, NaBH4, EtOH / 16 h / Ambient temperature 2: 94 percent / pyridine / 2 h / 0 °C 3: 83 percent / 18-crown-6 / dimethylsulfoxide / 3 h / 50 °C 4: 3.7 g / conc. HCl / tetrahydrofuran / 12 h / 100 °C 5: 4.75 percent / 1N NaOH / tetrahydrofuran / 4 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 50, # 31 p. 9457 - 9470
反应条件
1: 83 percent / 18-crown-6 / dimethylsulfoxide / 3 h / 50 °C 2: 3.7 g / conc. HCl / tetrahydrofuran / 12 h / 100 °C 3: 4.75 percent / 1N NaOH / tetrahydrofuran / 4 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 50, # 31 p. 9457 - 9470
