1,1',1''-(异氰基次甲基)三-苯合成路线 (共 8 条)
反应条件
1: triphenylmethylamine With 15-crown-5; sodium hydride in benzene T=40 - 50°C; 0.25 h; 2: chloroform in benzene T=40°C; 1 h;
参考文献
Bardsley, Kathryn; Hagigeorgiou, Michael; Lengyel, Istvan; Cesare, Victor
Synthetic Communications, 2013 , vol. 43, # 12 p. 1727 - 1733
反应条件
pyridine; p-toluenesulfonyl chloride 6 h; Ambient temperature;
参考文献
Zieger, Herman E.; Wo, Shiming
Journal of Organic Chemistry, 1994 , vol. 59, # 14 p. 3838 - 3840
反应条件
1: 48.9 percent / Et3N / CH2Cl2 2: 74 percent / NaOtBu / diethyl ether; tetrahydrofuran / 1 h / 0 °C 3: octane / 1 h / Heating View Scheme
参考文献
Lengyel, Istvan; Cesare, Victor; Adam, Ian; Taldone, Tony
Heterocycles, 2002 , vol. 57, # 1 p. 73 - 95
反应条件
1: 74 percent / NaOtBu / diethyl ether; tetrahydrofuran / 1 h / 0 °C 2: octane / 1 h / Heating View Scheme
参考文献
Lengyel, Istvan; Cesare, Victor; Adam, Ian; Taldone, Tony
Heterocycles, 2002 , vol. 57, # 1 p. 73 - 95
反应条件
in octane 2.75 h; Heating;
参考文献
Lengyel; Cesare; Karram; Taldone
Journal of Heterocyclic Chemistry, 2001 , vol. 38, # 4 p. 997 - 1002
反应条件
in octane 1 h; Heating;
参考文献
Lengyel, Istvan; Cesare, Victor; Adam, Ian; Taldone, Tony
Heterocycles, 2002 , vol. 57, # 1 p. 73 - 95
反应条件
in benzene
T=350°C; 0.00416667 h;
参考文献
Zieger, Herman E.; Wo, Shiming
Journal of Organic Chemistry, 1994 , vol. 59, # 14 p. 3838 - 3840
反应条件
in dichloromethane
T=0°C; 2 h;
参考文献
Zieger, Herman E.; Wo, Shiming
Journal of Organic Chemistry, 1994 , vol. 59, # 14 p. 3838 - 3840