4-碘-3-硝基-苯甲酰胺合成路线 (共 4 条)
反应条件
ammonia in methanol T=-15 - 25°C; 72 h;
参考文献
DIVI'S LABORATORIES LIMITED; Divi, Murali Krishna Prasad; Rao, Mysore Aswatha Narayana; Rajuri, Venkataramana
Patent: US2013/172618 A1, 2013 ;
Location in patent: Paragraph 0027; 0028 ;
反应条件
thionyl chloride in water; N,N-dimethyl-formamide; acetonitrile
参考文献
Octamer, Inc.
Patent: US5877185 A1, 1999 ;
反应条件
tributylphosphine; sodium iodide; niobium bromide in 1-methyl-pyrrolidin-2-one T=140°C; Finkelstein reaction; 18 h; Inert atmosphereMolecular sieveSealed tube;
参考文献
Cant, Alastair A.; Bhalla, Rajiv; Pimlott, Sally L.; Sutherland, Andrew
Chemical Communications, 2012 , vol. 48, # 33 p. 3993 - 3995
参考文献
Journal of Organic Chemistry, , vol. 62, # 10 p. 3093 - 3097