反式-1-苯基-1-戊烯合成路线 (共 108 条)
反应条件
(i) MCPBA, THF, (ii) LDA, (iii) /BRN= 1420755/; Multistep reaction;
参考文献
Reich,H.J. et al.
Journal of the American Chemical Society, 1979 , vol. 101, p. 6648 - 6656
反应条件
(i) LDA, (ii) /BRN= 1420755/, (iii) CH2Cl2; Multistep reaction;
参考文献
Reich,H.J.; Shah,S.K.
Journal of the American Chemical Society, 1975 , vol. 97, p. 3250 - 3252
反应条件
sodium hydride in N,N-dimethyl-formamide
Yield given. Yields of byproduct given;
参考文献
Buss, Antony D.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2307 - 2326
反应条件
in toluene
T=102°C; Further byproducts given;
参考文献
Doyle, Michael P.; High, Kenneth G.; Oon, Su-Min; Osborn, Antonio K.
Tetrahedron Letters, 1989 , vol. 30, # 23 p. 3049 - 3052
反应条件
in toluene
T=102°C; Further byproducts given;
参考文献
Doyle, Michael P.; High, Kenneth G.; Oon, Su-Min; Osborn, Antonio K.
Tetrahedron Letters, 1989 , vol. 30, # 23 p. 3049 - 3052
反应条件
24 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Smegal, John A.; Meier, Ingrid K.; Schwartz, Jeffrey
Journal of the American Chemical Society, 1986 , vol. 108, # 6 p. 1322 - 1323
反应条件
n-butyllithium
T=25°C; Yield given. Yields of byproduct given;
参考文献
Maryanoff, Bruce E.; Reitz, Allen B.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 27, p. 167 - 190
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane
-78 deg C, 3 h then rt., 1 h; Yield given. Yields of byproduct given;
参考文献
Baudin, J. B.; Hareau, G.; Julia, S. A.; Lorne, R.; Ruel, O.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, p. 856 - 878
反应条件
in tetrahydrofuran
T=-25°C; Product distribution;
参考文献
Reitz, Allen B.; Mutter, Martin S.; Maryanoff, Bruce E.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1873 - 1875
反应条件
in tetrahydrofuran
T=-25°C; Product distribution;
参考文献
Reitz, Allen B.; Mutter, Martin S.; Maryanoff, Bruce E.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1873 - 1875