hydrogenchloride in ethanol; water 0.5 h; Heating / reflux;
参考文献
Piotrowski, David W.; Rogers, Bruce N.; McWhorter JR., William W.; Walker, Daniel Patrick; Corbett, Jeffrey W.; Groppi JR., Vincent E.; Rudmann, Daniel G.
Patent: US2003/236287 A1, 2003 ;
Location in patent: Page 43, 44 ;
US 20030236287 A1
1: 89 percent / iron, acetic acid / H2O / 3 h / Heating 2: 80 percent / acetic acid / 0.25 h / 100 °C 3: 73 percent / conc. nitric acid, conc. H2SO4 / 0 °C 4: 57 percent / HCl / 1 h / Heating View Scheme
参考文献
Ahmad, Arshad; Dunbar, Linda J.; Green, Iain G.; Harvey, Ian W.; Shepherd, Thomas; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 19 p. 2751 - 2758
Ahmad, Arshad; Dunbar, Linda J.; Green, Iain G.; Harvey, Ian W.; Shepherd, Thomas; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 19 p. 2751 - 2758