1: 4-(3,4-dimethoxyphenyl)-3-buten-2-one With sodium hexamethyldisilazane in tetrahydrofuran T=-78°C; 0.5 h; 2: 3,4-dimethoxycinnamic acid chloride in tetrahydrofuran T=-78 - 20°C; 12 h;
参考文献
THE OHIO STATE UNIVERSITY RESEARCH FOUNDATION; LI, Pui-Kai; LI, Chenglong; LIN, Jiayuh; FUCHS, James, R.
Patent: WO2010/121007 A1, 2010 ;
Location in patent: Page/Page column 6; 17-18 ;
Changtam, Chatchawan; de Koning, Harry P.; Ibrahim, Hasan; Sajid, M. Sohail; Gould, Matthew K.; Suksamrarn, Apichart
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 3 p. 941 - 956
potassium carbonate in water; N,N-dimethyl-formamide
T=20°C; 18 h;
参考文献
THE OHIO STATE UNIVERSITY RESEARCH FOUNDATION; LI, Pui-Kai; LI, Chenglong; LIN, Jiayuh; FUCHS, James, R.
Patent: WO2010/121007 A1, 2010 ;
Location in patent: Page/Page column 5; 14-15 ;